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HomeMy WebLinkAboutMetals 03062024LA TESTING g.'A TESTING Noah Ambos CTEH Center for Toxicology & Env. Health 5120 North Shore Drive North Little Rock, AR 72118 LA Testing 5431 Industrial Drive Huntington Beach, CA 92649 (714) 828-4999 CustomerService(o)emsl.com Re: Narrative: NIOSH 7303 LA Testing Order: 332404002, Project ID: PROJ-032229 Dear Noah HUNTINGTON BEACH, CA 92649 5431 INDUSTRIAL DRIVE PHONE: (714) 828-4999 On 3/ 7/2024, LA Testing Huntington Beach, CA received 22 air samples for metals analysis via NIOSH 7300 Modified method. The samples were received and logged in following normal lab procedures. All samples were received under Chain of Custody and in good condition unless otherwise noted. NIOSH 7300 Modified LA Testing Order: 332404002, Project ID: PROJ-032229: All samples were prepared and analyzed according to the method specified NIOSH 7300 Modified. The samples were submitted on cellulose ester membrane filters which were prepared utilizing a hot block digestion technique as indicated in the method. The samples were then analyzed via Inductively Coupled Plasma (ICP) analysis utilizing Atomic Emission Spectroscopy (AES). All preparation and analyses were performed within the method specific hold time requirement. Results are reported in mg/m3. Quality Control Dilutions: None Calibrations: The RL, RLVS ICV and bracketing CCV standards were within control limits. Blanks: Target analytes were not detected above the reporting limit in the associated blanks. Media blank was not subtracted from sample concentrations. LCS/LCSD: The laboratory control sample spike recoveries and RPD results were within control limits. ICSA/ICSB: The interference check solution results were within control limits. QC was performed at rates compliant with both the American Industrial Hygiene Association (AIHA) and the California Environmental Laboratory Accreditation Program (ELAP). 1 certify that this report is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. In addition, I certify, that to the best of my knowledge and belief, the data as reported are true and accurate. Release of the data contained in this Michael Chapman, Laboratory Manager q• Paqe 1 Of March 14, 2024 CHEMMETALNARR.2.0 LA Testing 5431 Industrial Drive, Huntington Beach, CA 92649 Phone: (714) 828-4999 Fax: (714) 828-4944 Email: hblabOlatestinq.com TESTING Attn: Noah Ambos 3/14/2024 CTEH Center for Toxicology & Env. Health 5120 North Shore Drive North Little Rock, AR 72118 Phone: (501) 801-8500 Fax: (501) 614-2835 The following analytical report covers the analysis performed on samples submitted to LA Testing on 3/7/2024. The results are tabulated on the attached data pages for the following client designated project: Project ID: PROJ-032229 PROJ-032229 The reference number for these samples is EMSL Order #332404002. Please use this reference when calling about these samples. If you have any questions, please do not hesitate to contact me at (714) 828-4999. Approved By: Michael Chapman, Laboratory Manager AIHA LAP, LLC-IHLAP Accredited #101650 EMSL maintains liability limited to cost of analysis. Interpretation and use of test results are the responsibility of the client. This report relates only to the samples reported above, and may not be reproduced, except in full, without written approval by EMSL. EMSL bears no responsibility for sample collection activities or analytical method limitations. The report reflects the samples as received. Results are generated from the field sampling data (sampling volumes and areas, locations, etc.) provided by the client on the Chain of Custody. Samples are within quality control criteria and met method specifications unless otherwise noted. Page 1 of 16 Paqe 2 Of 32 LA Testing LA Testing Order: 332404002 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/7/2024 09:25 AM North Little Rock, AR 72118 Collected: 3/6/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0306ME001A Collected. 3/6/2024 Lab ID: 332404002-0001 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.071 0.071 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH Client Sample Description TUCA0306ME002A Collected. 3/6/2024 Lab ID: 332404002-0002 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.071 0.071 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/14/2024 5:05:31 PM Page 2 of 16 Paqe 3 Of 32 LA Testing LA Testing Order: 332404002 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/7/2024 09:25 AM North Little Rock, AR 72118 Collected: 3/6/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0306ME002A Collected. 3/6/2024 Lab ID: 332404002-0002 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH Client Sample Description TUCA0306ME003A Collected. 3/6/2024 Lab ID: 332404002-0003 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.071 0.071 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/14/2024 5:05:31 PM Page 3 of 16 Paqe 4 Of 32 LA Testing LA Testing Order: 332404002 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/7/2024 09:25 AM North Little Rock, AR 72118 Collected: 3/6/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0306ME004A Collected. 3/6/2024 Lab ID: 332404002-0004 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.071 0.071 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH Client Sample Description TUCA0306ME005A Collected. 3/6/2024 Lab ID: 332404002-0005 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.9 3.9 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.79 0.79 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.79 0.79 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.9 3.9 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.079 0.079 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.16 0.16 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.79 0.79 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.39 0.39 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.79 0.79 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.39 0.39 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.39 0.39 pg/m' 3/13/2024 CM 3/13/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/14/2024 5:05:31 PM Page 4 of 16 Paqe 5 Of 32 LA Testing LA Testing Order: 332404002 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/7/2024 09:25 AM North Little Rock, AR 72118 Collected: 3/6/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0306ME005A Collected. 3/6/2024 Lab ID: 332404002-0005 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.39 0.39 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.79 0.79 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.79 0.79 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.79 0.79 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.79 0.79 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.39 0.39 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.79 0.79 pg/m' 3/13/2024 CM 3/13/2024 TH Client Sample Description TUCA0306ME006A Collected. 3/6/2024 Lab ID: 332404002-0006 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.6 3.6 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.6 3.6 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.071 0.071 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Molybdenum <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/14/2024 5:05:31 PM Page 5 of 16 Paqe 6 Of 32 LA Testing LA Testing Order: 332404002 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/7/2024 09:25 AM North Little Rock, AR 72118 Collected: 3/6/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0306ME007A Collected. 3/6/2024 Lab ID: 332404002-0007 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.6 3.6 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.72 0.72 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.72 0.72 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.6 3.6 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.072 0.072 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.72 0.72 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.72 0.72 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Molybdenum <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.72 0.72 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.72 0.72 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.72 0.72 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.72 0.72 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.72 0.72 pg/m' 3/13/2024 CM 3/13/2024 TH Client Sample Description TUCA0306ME008A Collected. 3/6/2024 Lab ID: 332404002-0008 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <4.6 4.6 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.91 0.91 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.91 0.91 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <4.6 4.6 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.091 0.091 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.18 0.18 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.91 0.91 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.46 0.46 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.91 0.91 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.46 0.46 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.46 0.46 pg/m' 3/13/2024 CM 3/13/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/14/2024 5:05:31 PM Page 6 of 16 Paqe 7 Of 32 LA Testing LA Testing Order: 332404002 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/7/2024 09:25 AM North Little Rock, AR 72118 Collected: 3/6/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0306ME008A Collected. 3/6/2024 Lab ID: 332404002-0008 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.46 0.46 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.91 0.91 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.91 0.91 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.91 0.91 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.91 0.91 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.46 0.46 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.91 0.91 pg/m' 3/13/2024 CM 3/13/2024 TH Client Sample Description TUCA0306ME009A Collected. 3/6/2024 Lab ID: 332404002-0009 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.6 3.6 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.6 3.6 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.071 0.071 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Molybdenum <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/14/2024 5:05:31 PM Page 7 of 16 Paqe 8 Of 32 LA Testing LA Testing Order: 332404002 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/7/2024 09:25 AM North Little Rock, AR 72118 Collected: 3/6/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0306ME010A Collected. 3/6/2024 Lab ID: 332404002-0010 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.6 3.6 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.6 3.6 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.071 0.071 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Molybdenum <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.36 0.36 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.71 0.71 pg/m' 3/13/2024 CM 3/13/2024 TH Client Sample Description TUCA0306MEFBO01A Collected. 3/6/2024 Lab ID: 332404002-0011 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <5.0 5.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <5.0 5.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.10 0.10 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.20 0.20 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.50 0.50 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.50 0.50 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.50 0.50 pg/filter 3/13/2024 CM 3/13/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/14/2024 5:05:31 PM Page 8 of 16 Paqe 9 Of 32 LA Testing LA Testing Order: 332404002 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/7/2024 09:25 AM North Little Rock, AR 72118 Collected: 3/6/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0306MEFBO01A Collected. 3/6/2024 Lab ID: 332404002-0011 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.50 0.50 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.50 0.50 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH Client Sample Description TUCA0306ME001 B Collected. 3/6/2024 Lab ID: 332404002-0012 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.069 0.069 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/14/2024 5:05:31 PM Page 9 of 16 Paqe 10 Of 32 LA Testing LA Testing Order: 332404002 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/7/2024 09:25 AM North Little Rock, AR 72118 Collected: 3/6/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0306ME002B Collected. 3/6/2024 Lab ID: 332404002-0013 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.4 3.4 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.4 3.4 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.069 0.069 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Molybdenum <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH Client Sample Description TUCA0306ME003B Collected. 3/6/2024 Lab ID: 332404002-0014 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.4 3.4 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.4 3.4 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.069 0.069 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/14/2024 5:05:31 PM Page 10 of 16 Paqe 11 Of 32 LA Testing LA Testing Order: 332404002 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/7/2024 09:25 AM North Little Rock, AR 72118 Collected: 3/6/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0306ME003B Collected. 3/6/2024 Lab ID: 332404002-0014 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH Client Sample Description TUCA0306ME004B Collected. 3/6/2024 Lab ID: 332404002-0015 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.069 0.069 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/14/2024 5:05:31 PM Page 11 of 16 Paqe 12 Of 32 LA Testing LA Testing Order: 332404002 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/7/2024 09:25 AM North Little Rock, AR 72118 Collected: 3/6/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0306ME005B Collected. 3/6/2024 Lab ID: 332404002-0016 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <4.4 4.4 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.87 0.87 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.87 0.87 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <4.4 4.4 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.087 0.087 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.17 0.17 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.87 0.87 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.44 0.44 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.87 0.87 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.44 0.44 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.44 0.44 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Molybdenum <0.44 0.44 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.87 0.87 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.87 0.87 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.87 0.87 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.87 0.87 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.44 0.44 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.87 0.87 pg/m' 3/13/2024 CM 3/13/2024 TH Client Sample Description TUCA0306ME006B Collected. 3/6/2024 Lab ID: 332404002-0017 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.4 3.4 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.4 3.4 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.068 0.068 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/14/2024 5:05:31 PM Page 12 of 16 Paqe 13 Of 32 LA Testing LA Testing Order: 332404002 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/7/2024 09:25 AM North Little Rock, AR 72118 Collected: 3/6/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0306ME006B Collected. 3/6/2024 Lab ID: 332404002-0017 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH Client Sample Description TUCA0306ME007B Collected. 3/6/2024 Lab ID: 332404002-0018 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.4 3.4 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.4 3.4 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.069 0.069 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Molybdenum <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/14/2024 5:05:31 PM Page 13 of 16 Paqe 14 Of 32 LA Testing LA Testing Order: 332404002 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/7/2024 09:25 AM North Little Rock, AR 72118 Collected: 3/6/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0306ME008B Collected. 3/6/2024 Lab ID: 332404002-0019 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.4 3.4 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.4 3.4 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.068 0.068 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Molybdenum <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.68 0.68 pg/m' 3/13/2024 CM 3/13/2024 TH Client Sample Description TUCA0306ME009B Collected. 3/6/2024 Lab ID: 332404002-0020 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.069 0.069 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/14/2024 5:05:31 PM Page 14 of 16 Paqe 15 Of 32 LA Testing LA Testing Order: 332404002 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/7/2024 09:25 AM North Little Rock, AR 72118 Collected: 3/6/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0306ME009B Collected. 3/6/2024 Lab ID: 332404002-0020 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH Client Sample Description TUCA0306ME010B Collected. 3/6/2024 Lab ID: 332404002-0021 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.4 3.4 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <3.4 3.4 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.069 0.069 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Molybdenum <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.34 0.34 pg/m' 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <0.69 0.69 pg/m' 3/13/2024 CM 3/13/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/14/2024 5:05:31 PM Page 15 of 16 Paqe 16 Of 32 LA Testing LA Testing Order: 332404002 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/7/2024 09:25 AM North Little Rock, AR 72118 Collected: 3/6/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0306MEFBO01 B Collected. 3/6/2024 Lab ID: 332404002-0022 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <5.0 5.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Antimony <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Arsenic <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Barium <5.0 5.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Beryllium <0.10 0.10 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Cadmium <0.20 0.20 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Chromium <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Cobalt <0.50 0.50 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Copper <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Lead <0.50 0.50 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Manganese <0.50 0.50 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Molybdenum <0.50 0.50 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Nickel <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Selenium <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Silver <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Thallium <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Vanadium <0.50 0.50 pg/filter 3/13/2024 CM 3/13/2024 TH 7300 Modified Zinc <1.0 1.0 pg/filter 3/13/2024 CM 3/13/2024 TH AIHA LAP, LLC-IHLAP Accredited #101650 Definitions: MDL - method detection limit J - Result was below the reporting limit, but at or above the MDL ND - indicates that the analyte was not detected at the reporting limit RL - Reporting Limit (Analytical) D - Dilution Sample required a dilution which was used to calculate final results ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/14/2024 5:05:31 PM Page 16 of 16 Paqe 17 Of 32 Printed: 3/14/2024 Batch: 33Q240313-1 MICE Instrument: 33-PE8300 Initial Cal Std: Cal Check Std: Internal Std: LCS Std MS Std Matrix: Cassettes I ICP QC Batch Summary Created: 3/13/24 12:34 pm By: camartinez Samples 332404002-0001 332404002-0005 332404002-0009 332404002-0013 332404002-0017 332404002-0002 332404002-0006 332404002-0010 332404002-0014 332404002-0018 332404002-0003 332404002-0007 332404002-0011 332404002-0015 332404002-0019 332404002-0004 332404002-0008 332404002-0012 332404002-0016 332404002-0020 Blank/DL Control Other Method Blank[7] Matrix Blank[7] LCS[1] LCSD[1] 332404002-0002 03/13/2411:53 03/13/2412:09 03/13/2411:58 03/13/2412:00 03/13/2412:22 Result Ng/filter RL Ng/filter IL Result pg/filter RL Ng/filter Result pg/filter True Conc jig/filter % Rec 73.7051-119. 552 Result pg/filter True Conc jig/filter % Rec 73.7051-119. 552 % RPD <m20 RL pg/m' Result Ng/m' Aluminum 0.675 5.0 0.305 5.0 23.6 25.0 94.5 24.7 25.0 98.8 4.49 3.5 0.95 Antimony 0.570 1.0 0.690 1.0 24.9 25.0 99.5 24.6 25.0 98.2 1.33 0.71 0.55 Arsenic -0.16 1. -0.455, 1.0 22.8 25.0 91.4 22.7 25.0 90.8 0.659 0.71 -0.059 Barium -0.010 5. 0.0 5.0 23.1 25. 92.3123.4 25.0 93.6 1.48, 3.5 0.042 Beryllium 0.0050 0.1 0.0050 0.1 23.3 25. 93.0 22.7 25.0 90.7 2.53 0.071 0.0035 Cadmium 0.010 0.2 -0.0050 0.2 25.3 25. 101 24.8 25.0 99.0 2.36 0.14 0.0 Chromium 0.0 1. -0.015 1. 24.3 25. 97.1 24.4 25.0 97.8 0.698 0.71 0.0141 Cobalt 0.0200 0.50 0.025 0.5 26.1 25. 104 25.4 25.0 102 2.51 0.35 0.010 Copper -0.26 1. -0.34 1. 25.1 25. 100 25.5 25.0 102 1.70 0.71 0.091 Lead -0.085 0.5 -0.23 0.50 24.6 25. 98.3 23.9 25.0 95.7 2.74 0.35 0.0 Manganese -0.0050 0.5 -0.0050 0.50 24.1 25. 96.2 24.5 25.0 98.0 1.85 0.35 0.031 Molybdenum -0.0250 0.50 0.015 0.50 25.6 25.0 102 25.1 25.0 100 1.98 0.35 0.0141 Nickel -0.010 1. -0.0050 1.0 24.3 25. 97.2 25.8 25.0 103 5.89 0.71 0.035 Selenium 0.205 1. -0.430 1.0 23.5 25. 94.1 22.8 25.0 91.2 3.15 0.71 0.017 Silver 0.0350 1.0 0.060 1. 24.2 25.q 97.q 24.6 25.0 98.3 1.3q 0.71 0.0035 Thallium -0.0950 1.0 0.090 1. 25.3 25. 101 24.4 25.0 97.7 3.36 0.71 -0.038 Vanadium 0.0100 0.5 -0.0050 0.5 24.5 25. 97.9 24.8 25.0 99.4 1.52 0.35 0.0035 Zinc -0.030 1. -0.10 1. 26.q 25. 104 25.4 25.0 101 2.28 0.71 0.091 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 1 of 4 Page 18 Of 32 Printed: 3/14/2024 Batch: 33Q240313-1 MCE Instrument: 33-PE8300 Initial Cal Std: Cal Check Std: Internal Std: LCS Std MS Std Matrix: Cassettes ICP QC Batch Summary Created: 3/13/24 12:34 pm By: camartinez Samples: 332404002-0001 332404002-0002 332404002-0003 332404002-0004 332404002-0005 332404002-0009 332404002-0006 332404002-0010 332404002-0007 332404002-0011 332404002-0008 332404002-0012 332404002-0013 332404002-0017 332404002-0014 332404002-0018 332404002-0015 332404002-0019 332404002-0016 332404002-0020 Other 332404002-0003 332404002-0004 332404002-0005 332404002-0007 332404002-0009 332404002-0011 332404002-0001 03/13/2412:24 03/13/2412:27 03/13/2412:29 03/13/2412:38 03/13/2412:43 03/13/2412:47 03/13/2412:54 RL pg/m3 Result pg/m3 RL pg/m' Result pg/m3 RL pg/m' Result pg/ma RL pg/m' Result pg/ma RL pg/m' Result pg/ma RL pg/filter Result pg/filter RL pg/m3 Result pg/m' Aluminum 3.5 0.92 3.5 0.876 3. 0.720 3.6 1.05 3.6 0.877 5.0 0.790 3.5 0.60 Antimony 0.71 0.181 0.71 0.542 0.7 -0.0551 0.72 0.687 0.71 0.353 1.0 0.245 0.71 0.521 Arsenic 0.71 -0.074 0.71 -0.103 0.7 0.0275 0.72 -0.157 0.71 -0.289 1.0 0.0950 0.71 0.0070 Barium 3.5 0.039 3.5 0.0390 3. 0.0472 3.6 0.0358 3.6 0.0321 5.0 0.0300 3.5 0.035 Beryllium 0.071 0.0035 0.071 0.00 0.07 0.00393 0.072 0.00358 0.071 0.00356 0.10 0.00 0.071 0.0035 Cadmium 0.14 0.00355 0.14 0.0142 0.1 0.00787 0.14 0.00715 0.14 0.00 0.20 0.00500 0.14 0.0035 Chromium 0.71 0.0355 0.71 0.0177 0.7 0.232 0.72 0.0286 0.71 0.0214 1.0 0.0250 0.71 0.035 Cobalt 0.3 0.0177 0.35 0.0248 0.3 0.0197 0.36 0.00358 0.36 0.0107 0.50 0.0200 0.3 0.024 Copper 0.71 0.0674 0.71 0.0709 0.7 0.0551 0.72 0.0715 0.71 0.0784 1.q 0.0350 0.71 0.042 Lead 0.35 0.00 0.3 -0.056 0.3 -0.027 0.36 -0.0250 0.36 -0.0107 0.5 -0.140 0.3 -0.028 Manganese 0.35 0.0213 0.3q 0.0248 0.3 0.0236 0.36 0.0179 0.36 0.0214 0.50 0.0550 0.35 0.021 Molybdenum 0.35 0.00355 0.35 0.0390 0.3 -0.00393 0.36 0.0107 0.36 -0.0143 0.50 0.0250 0.3 -0.031 Nickel 0.71 0.0177 0.71 0.0248 0.7E 0.0275 0.72 0.0250 0.71 0.0250 1.0 0.0250 0.71 0.021 Selenium 0.71 -0.167 0.71 -0.10 0.7 0.161 0.72 0.0966 0.71 0.0107 1.0 0.0100 0.71 0.085 Silver 0.71 0.0177 0.71 0.024 0.7 0.0433 0.72 0.0394 0.71 0.0392 1.01 0.00500 0.71 0.024 Thallium 0.71 -0.121 0.71 -0.078 0.7 -0.070 0.72 -0.0250 0.71 -0.146 1.0 -0.145 0.71 -0.063 Vanadium 0.35 0.00351 0.31 0.0070 0.3 0.00393 0.36 0.00 0.36 -0.0214 0.50 -0.010 0.3 -0.014 Zinc 0.71 0.0810 0.711 0.070 0.7 0.0708 0.72 0.0823 0.71 0.107 1.01 0.10q 0.71 0.074 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 2 of 4 Page 19 Of 32 Printed: 3/14/2024 ICP QC Batch Summary Batch: 33Q240313-1 MICE Created: 3/13/24 12:34 pm By: camartinez Instrument: 33-PE8300 Initial Cal Std: Samples: Cal Check Std: Internal Std: 332404002-0001 332404002-0005 332404002-0009 LCS Std 332404002-0002 332404002-0006 332404002-0010 332404002-0003 332404002-0007 332404002-0011 MS Std 332404002-0004 332404002-0008 332404002-0012 Matrix: Cassettes 332404002-0013 332404002-0017 332404002-0014 332404002-0018 332404002-0015 332404002-0019 332404002-0016 332404002-0020 Other 332404002-0010 332404002-0006 332404002-0012 332404002-0013 332404002-0015 332404002-0018 332404002-0020 03/13/2413:03 03/13/2413:06 03/13/2413:08 03/13/2413:10 03/13/2413:15 03/13/2413:22 03/13/2413:31 RL pg/m' Result Ng/m' RL pg/m' Result Ng/m' RL pg/m' Result Ng/m' RL pg/m' Result pg/m' RL pg/m' Result Ng/m' RL pg/m' Result pg/m' RL pg/m' Result pg/m' Aluminum 3.6 0.416 3.6 0.618 3.5 0.770 3.4 0.345 3.5 0.478 3.4 0.746 3.5 0.54 Antimony 0.71 0.552 0.71 0.568 0.69 0.628 0.69 0.555 0.69 0.633 0.69 0.241 0.69 0.24 Arsenic 0.71 -0.196 0.71 0.0393 0.6 -0.242 0.69 -0.0483 0.69 -0.197 0.69 0.0310 0.6 -0.271 Barium 3.6 0.0178 3.6 0.0393 3.5 0.0207 3.4 0.0276 3.5 0.0104 3. 0.0241 3.5 0.020 Beryllium 0.071 0.00356 0.071 0.00 0.069 0.00 0.069 0.00 0.069 0.00346 0.06 0.00 0.069 0.0034 Cadmium 0.14 0.0107 0.14 0.00 0.14 0.00 0.14 0.00690 0.14 0.0104 0.14 0.0103 0.14 0.010 Chromium 0.71 0.0142 0.71 0.207 0.69 0.190 0.69 0.0448 0.69 0.00 0.69 0.0482 0.69 0.031 Cobalt 0.36 0.00356 0.36 0.0179 0.3 -0.00345 0.34 0.0138 0.3 -0.00692 0.34 0.0138 0.35 0.020 Copper 0.71 0.0285 0.711 0.0464 0.69 0.0104 0.6p 0.0172 0.69 0.0138 0.69 0.0138 0.69 0.027 Lead 0.3 -0.0676 0.36 0.0464 0.3 -0.100 0.34 -0.107 0.3 -0.0104 0.3 -0.086 0.3 -0.017 Manganese 0.36 0.0427 0.36 0.0250 0.35 0.0138 0.34 0.0241 0.35 0.0138 0.31 0.0172 0.35 0.013 Molybdenum 0.36 0.0142 0.36 0.0143 0.3 -0.0138 0.34 0.00345 0.35 0.0173 0.3 -0.0172 0.35 0.0034 Nickel 0.71 0.0320 0.71 0.0250 0.6q 0.0207 0.69 0.0310 0.69 0.0173 0.69 0.426 0.69 0.038 Selenium 0.71 -0.189 0.71 -0.060 0.6 -0.104 0.69 0.141 0.69 0.0485 0.69 0.0963 0.6 -0.13 Silver 0.71 0.0285 0.71 0.0179 0.6 0.0276 0.69 0.0310 0.69 -0.00346 0.69 0.0310 0.69 0.020 Thallium 0.71 -0.067 0.71 -0.20 0.6 -0.0311 0.69 -0.0483 0.69 -0.194 0.69 0.107 0.6 -0.024 Vanadium 0.3 -0.00712 0.36 0.00 0.3 0.0034 0.34 -0.00345 0.3 -0.0138 0.341 0.00 0.3 -0.010 Zinc 0.71 0.0783 0.71 0.0893 0.6 0.0622 0.69 0.0621 0.69 0.0346 0.60 0.0447 0.60 0.0521 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 3 of 4 Page 20 Of 32 Printed: 3/14/2024 Batch: 33Q240313-1 MCE Instrument: 33-PE8300 Initial Cal Std: Cal Check Std: Internal Std: LCS Std MS Std Matrix: Cassettes ICP QC Batch Summary Created: 3/13/24 12:34 pm By: camartinez Samples: 332404002-0001 332404002-0002 332404002-0003 332404002-0004 332404002-0005 332404002-0009 332404002-0006 332404002-0010 332404002-0007 332404002-0011 332404002-0008 332404002-0012 332404002-0013 332404002-0017 332404002-0014 332404002-0018 332404002-0015 332404002-0019 332404002-0016 332404002-0020 Other 332404002-0008 332404002-0014 332404002-0016 332404002-0017 332404002-0019 03/13/2414:09 03/13/2414:11 03/13/2414:14 03/13/2414:16 03/13/2414:23 RL pg/m3 Result pg/m' RL pg/m' Result pg/m' RL pg/m' Result pg/m' RL pg/m' Result pg/m' RL pg/m' Result pg/m' Aluminum 4.6 0.939 3.4 0.816 4.4 0.236 3.4 0.516 3.4 0.386 Antimony 0.91 0.716 0.69 0.685 0.87 0.720 0.68 0.581 0.68 0.437 Arsenic 0.91 -0.109 0.6 -0.196 0.8 -0.140 0.68 -0.0137 0.68 -0.140 Barium 4.6 0.0410 3.4 0.0344 4.4 0.00873 3.4 0.0273 3.4 0.0171 Beryllium 0.091 0.00456 0.069 0.00344 0.087 0.00437 0.068 0.00 0.06 0.00 Cadmium 0.18 0.0182 0.14 0.00 0.17 0.0218 0.14 0.00 0.14 0.0102 Chromium 0.91 0.0319 0.69 0.0586 0.87 0.0131 0.68 0.0410 0.68 0.020 Cobalt 0.46 0.0273 0.34 0.00689 0.44 0.0218 0.3 -0.0103 0.34 -0.00341 Copper 0.91 -0.018 0.6 -0.044 0.8 -0.043 0.6 -0.047 0.6 -0.130 Lead 0.46 0.00 0.3 -0.037 0.4 -0.017 0.3 -0.0684 0.34 -0.0273 Manganese 0.46 0.0273 0.34 0.0172 0.44 0.0131 0.34 0.0137 0.34 0.00683 Molybdenum 0.46 0.0273 0.3 -0.0068 0.4 -0.00437 0.34 0.0171 0.34 0.030 Nickel 0.91 0.0365 0.69 0.0344 0.87 0.0218 0.68 0.431 0.68 0.023 Selenium 0.91 -0.210 0.69 0.117 0.8 -0.131 0.68 0.0308 0.68 0.0376 Silver 0.91 -0.00456 0.6q 0.0q 0.87 0.00 0.68 0.00684 0.68 0.047 Thallium 0.91 -0.278 0.6 -0.145 0.8 -0.122 0.68 -0.154 0.68 -0.143 Vanadium 0.46 0.00456 0.34 0.0276 0.4 -0.00437 0.34 0.0200 0.34 0.013 Zinc 0.91 0.0775 0.69 0.0689 0.871 0.0611 0.68 0.0615 0.68 -0.020 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 4 of 4 Page 21 Of 32 Printed: 3/14/2024 Batch: 33Q240313-1 MICE Instrument: 33-PE8300 Initial Cal Std: Cal Check Std: Internal Std: LCS Std MS Std Matrix: Cassettes I ICP QC Batch Summary Created: 3/13/24 12:34 pm By: camartinez Samples 332404002-0001 332404002-0005 332404002-0009 332404002-0013 332404002-0017 332404002-0002 332404002-0006 332404002-0010 332404002-0014 332404002-0018 332404002-0003 332404002-0007 332404002-0011 332404002-0015 332404002-0019 332404002-0004 332404002-0008 332404002-0012 332404002-0016 332404002-0020 Blank/DL Control Other Method Blank[7] Matrix Blank[7] LCS[1] LCSD[1] 332404002-0002 03/13/2411:53 03/13/2412:09 03/13/2411:58 03/13/2412:00 03/13/2412:22 Result Ng/filter RL Ng/filter IL Result pg/filter RL Ng/filter Result pg/filter True Conc jig/filter % Rec 73.7051-119. 552 Result pg/filter True Conc jig/filter % Rec 73.7051-119. 552 % RPD <m20 RL pg/m' Result Ng/m' Aluminum 0.675 5.0 0.305 5.0 23.6 25.0 94.5 24.7 25.0 98.8 4.49 3.5 0.95 Antimony 0.570 1.0 0.690 1.0 24.9 25.0 99.5 24.6 25.0 98.2 1.33 0.71 0.55 Arsenic -0.16 1. -0.455, 1.0 22.8 25.0 91.4 22.7 25.0 90.8 0.659 0.71 -0.059 Barium -0.010 5. 0.0 5.0 23.1 25. 92.3123.4 25.0 93.6 1.48, 3.5 0.042 Beryllium 0.0050 0.1 0.0050 0.1 23.3 25. 93.0 22.7 25.0 90.7 2.53 0.071 0.0035 Cadmium 0.010 0.2 -0.0050 0.2 25.3 25. 101 24.8 25.0 99.0 2.36 0.14 0.0 Chromium 0.0 1. -0.015 1. 24.3 25. 97.1 24.4 25.0 97.8 0.698 0.71 0.0141 Cobalt 0.0200 0.50 0.025 0.5 26.1 25. 104 25.4 25.0 102 2.51 0.35 0.010 Copper -0.26 1. -0.34 1. 25.1 25. 100 25.5 25.0 102 1.70 0.71 0.091 Lead -0.085 0.5 -0.23 0.50 24.6 25. 98.3 23.9 25.0 95.7 2.74 0.35 0.0 Manganese -0.0050 0.5 -0.0050 0.50 24.1 25. 96.2 24.5 25.0 98.0 1.85 0.35 0.031 Molybdenum -0.0250 0.50 0.015 0.50 25.6 25.0 102 25.1 25.0 100 1.98 0.35 0.0141 Nickel -0.010 1. -0.0050 1.0 24.3 25. 97.2 25.8 25.0 103 5.89 0.71 0.035 Selenium 0.205 1. -0.430 1.0 23.5 25. 94.1 22.8 25.0 91.2 3.15 0.71 0.017 Silver 0.0350 1.0 0.060 1. 24.2 25.q 97.q 24.6 25.0 98.3 1.3q 0.71 0.0035 Thallium -0.0950 1.0 0.090 1. 25.3 25. 101 24.4 25.0 97.7 3.36 0.71 -0.038 Vanadium 0.0100 0.5 -0.0050 0.5 24.5 25. 97.9 24.8 25.0 99.4 1.52 0.35 0.0035 Zinc -0.030 1. -0.10 1. 26.q 25. 104 25.4 25.0 101 2.28 0.71 0.091 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 1 of 4 Page 22 Of 32 Printed: 3/14/2024 ICP QC Batch Summary Batch: 33Q240313-1 MICE Created: 3/13/24 12:34 pm By: camartinez Instrument: 33-PE8300 Initial Cal Std: Samples: Cal Check Std: Internal Std: 332404002-0001 332404002-0005 332404002-0009 LCS Std 332404002-0002 332404002-0006 332404002-0010 332404002-0003 332404002-0007 332404002-0011 MS Std 332404002-0004 332404002-0008 332404002-0012 Matrix: Cassettes 332404002-0013 332404002-0017 332404002-0014 332404002-0018 332404002-0015 332404002-0019 332404002-0016 332404002-0020 Other 332404002-0003 332404002-0004 332404002-0005 332404002-0007 332404002-0009 332404002-0011 332404002-0001 03/13/2412:24 03/13/2412:27 03/13/2412:29 03/13/2412:38 03/13/2412:43 03/13/2412:47 03/13/2412:54 RL pg/m' Result Ng/m3 RL pg/m' Result Ng/m' RL pg/m' Result Ng/m' RL pg/m' Result pg/m' RL pg/m' Result Ng/m' RL pg/filter Result Ng/filter RL pg/m' Result Ng/m3 Aluminum 3.5 0.929 3.5 0.876 3. 0.720 3.6 1.05 3.6 0.877 5.0 0.790 3.5 0.60 Antimony 0.71 0.181 0.71 0.542 0.7 -0.0551 0.72 0.687 0.71 0.353 1.0 0.245 0.71 0.521 Arsenic 0.71 -0.0745 0.71 -0.103 0.7 0.0275 0.72 -0.157 0.71 -0.289 1.0 0.0950 0.71 0.0070 Barium 3.5 0.0390 3.5 0.0390 3. 0.0472 3.6 0.0358 3.6 0.0321 5.0 0.0300 3.5 0.035 Beryllium 0.071 0.00355 0.071 0.00 0.07 0.00393 0.072 0.00358 0.071 0.00356 0.10 0.00 0.071 0.0035 Cadmium 0.14 0.00355 0.14 0.0142 0.1 0.00787 0.14 0.00715 0.14 0.00 0.20 0.00500 0.11 0.0035 Chromium 0.71 0.0355 0.71 0.0177 0.7 0.232 0.72 0.0286 0.71 0.0214 1.0 0.0250 0.71 0.035 Cobalt 0.35 0.0177 0.35 0.0248 0.3 0.0197 0.36 0.00358 0.36 0.0107 0.50 0.0200 0.35 0.024 Copper 0.71 0.0674 0.71 0.0709 0.7 0.0551 0.72 0.0715 0.71 0.0784 1.q 0.0350 0.71 0.042 Lead 0.35 0.00 0.3 -0.056 0.3 -0.027 0.36 -0.0250 0.36 -0.0107 0.5 -0.140 0.3 -0.028 Manganese 0.35 0.0213 0.35 0.0248 0.3 0.0236 0.36 0.0179 0.36 0.0214 0.50 0.0550 0.35 0.021 Molybdenum 0.35 0.00355 0.35 0.0390 0.3 -0.00393 0.36 0.0107 0.36 -0.0143 0.50 0.0250 0.3 -0.031 Nickel 0.71 0.0177 0.71 0.0248 0.7E 0.0275 0.72 0.0250 0.71 0.0250 1.0 0.0250 0.71 0.021 Selenium 0.71 -0.167 0.71 -0.10 0.7 0.161 0.72 0.0966 0.71 0.0107 1.0 0.0100 0.71 0.085 Silver 0.71 0.0177 0.71 0.024 0.7 0.0433 0.72 0.0394 0.71 0.0392 1.01 0.00500 0.71 0.024 Thallium 0.71 -0.121 0.71 -0.078 0.7 -0.070 0.72 -0.0250 0.71 -0.146 1.0 -0.145 0.71 -0.063 Vanadium 0.35 0.00355 0.35 0.0070 0.3 0.00393 0.36 0.00 0.36 -0.0214 0.50 -0.010 0.3 -0.014 Zinc 0.71 0.0816 0.71 0.070 0.7 0.0708 0.72 0.0823 0.71 0.107 1.0 0.100 0.711 0.074 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 2 of 4 Page 23 Of 32 Printed: 3/14/2024 ICP QC Batch Summary Batch: 33Q240313-1 MICE Created: 3/13/24 12:34 pm By: camartinez Instrument: 33-PE8300 Initial Cal Std: Samples: Cal Check Std: Internal Std: 332404002-0001 332404002-0005 332404002-0009 LCS Std 332404002-0002 332404002-0006 332404002-0010 332404002-0003 332404002-0007 332404002-0011 MS Std 332404002-0004 332404002-0008 332404002-0012 Matrix: Cassettes 332404002-0013 332404002-0017 332404002-0014 332404002-0018 332404002-0015 332404002-0019 332404002-0016 332404002-0020 Other 332404002-0010 332404002-0006 332404002-0012 332404002-0013 332404002-0015 332404002-0018 332404002-0020 03/13/2413:03 03/13/2413:06 03/13/2413:08 03/13/2413:10 03/13/2413:15 03/13/2413:22 03/13/2413:31 RL pg/m' Result Ng/m' RL pg/m' Result Ng/m' RL pg/m' Result Ng/m' RL pg/m' Result pg/m' RL pg/m' Result Ng/m' RL pg/m' Result pg/m' RL pg/m' Result pg/m' Aluminum 3.6 0.416 3.6 0.618 3.5 0.770 3.4 0.345 3.5 0.478 3.4 0.746 3.5 0.54 Antimony 0.71 0.552 0.71 0.568 0.69 0.628 0.69 0.555 0.69 0.633 0.69 0.241 0.69 0.24 Arsenic 0.71 -0.196 0.71 0.0393 0.6 -0.242 0.69 -0.0483 0.69 -0.197 0.69 0.0310 0.6 -0.271 Barium 3.6 0.0178 3.6 0.0393 3.5 0.0207 3.4 0.0276 3.5 0.0104 3. 0.0241 3.5 0.020 Beryllium 0.071 0.00356 0.071 0.00 0.069 0.00 0.069 0.00 0.069 0.00346 0.06 0.00 0.069 0.0034 Cadmium 0.14 0.0107 0.14 0.00 0.14 0.00 0.14 0.00690 0.14 0.0104 0.14 0.0103 0.14 0.010 Chromium 0.71 0.0142 0.71 0.207 0.69 0.190 0.69 0.0448 0.69 0.00 0.69 0.0482 0.69 0.031 Cobalt 0.36 0.00356 0.36 0.0179 0.3 -0.00345 0.34 0.0138 0.3 -0.00692 0.34 0.0138 0.35 0.020 Copper 0.71 0.0285 0.711 0.0464 0.69 0.0104 0.6p 0.0172 0.69 0.0138 0.69 0.0138 0.69 0.027 Lead 0.3 -0.0676 0.36 0.0464 0.3 -0.100 0.34 -0.107 0.3 -0.0104 0.3 -0.086 0.3 -0.017 Manganese 0.36 0.0427 0.36 0.0250 0.35 0.0138 0.34 0.0241 0.35 0.0138 0.31 0.0172 0.35 0.013 Molybdenum 0.36 0.0142 0.36 0.0143 0.3 -0.0138 0.34 0.00345 0.35 0.0173 0.3 -0.0172 0.35 0.0034 Nickel 0.71 0.0320 0.71 0.0250 0.6q 0.0207 0.69 0.0310 0.69 0.0173 0.69 0.426 0.69 0.038 Selenium 0.71 -0.189 0.71 -0.060 0.6 -0.104 0.69 0.141 0.69 0.0485 0.69 0.0963 0.6 -0.13 Silver 0.71 0.0285 0.71 0.0179 0.6 0.0276 0.69 0.0310 0.69 -0.00346 0.69 0.0310 0.69 0.020 Thallium 0.71 -0.067 0.71 -0.20 0.6 -0.0311 0.69 -0.0483 0.69 -0.194 0.69 0.107 0.6 -0.024 Vanadium 0.3 -0.00712 0.36 0.00 0.3 0.0034 0.34 -0.00345 0.3 -0.0138 0.341 0.00 0.3 -0.010 Zinc 0.71 0.0783 0.71 0.0893 0.6 0.0622 0.69 0.0621 0.69 0.0346 0.60 0.0447 0.60 0.0521 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 3 of 4 Page 24 Of 32 Printed: 3/14/2024 Batch: 33Q240313-1 MCE Instrument: 33-PE8300 Initial Cal Std: Cal Check Std: Internal Std: LCS Std MS Std Matrix: Cassettes ICP QC Batch Summary Created: 3/13/24 12:34 pm By: camartinez Samples: 332404002-0001 332404002-0002 332404002-0003 332404002-0004 332404002-0005 332404002-0009 332404002-0006 332404002-0010 332404002-0007 332404002-0011 332404002-0008 332404002-0012 332404002-0013 332404002-0017 332404002-0014 332404002-0018 332404002-0015 332404002-0019 332404002-0016 332404002-0020 Other 332404002-0008 332404002-0014 332404002-0016 332404002-0017 332404002-0019 03/13/2414:09 03/13/2414:11 03/13/2414:14 03/13/2414:16 03/13/2414:23 RL pg/m3 Result pg/m' RL pg/m' Result pg/m' RL pg/m' Result pg/m' RL pg/m' Result pg/m' RL pg/m' Result pg/m' Aluminum 4.6 0.939 3.4 0.816 4.4 0.236 3.4 0.516 3.4 0.386 Antimony 0.91 0.716 0.69 0.685 0.87 0.720 0.68 0.581 0.68 0.437 Arsenic 0.91 -0.109 0.6 -0.196 0.8 -0.140 0.68 -0.0137 0.68 -0.140 Barium 4.6 0.0410 3.4 0.0344 4.4 0.00873 3.4 0.0273 3.4 0.0171 Beryllium 0.091 0.00456 0.069 0.00344 0.087 0.00437 0.068 0.00 0.06 0.00 Cadmium 0.18 0.0182 0.14 0.00 0.17 0.0218 0.14 0.00 0.14 0.0102 Chromium 0.91 0.0319 0.69 0.0586 0.87 0.0131 0.68 0.0410 0.68 0.020 Cobalt 0.46 0.0273 0.34 0.00689 0.44 0.0218 0.3 -0.0103 0.34 -0.00341 Copper 0.91 -0.018 0.6 -0.044 0.8 -0.043 0.6 -0.047 0.6 -0.130 Lead 0.46 0.00 0.3 -0.037 0.4 -0.017 0.3 -0.0684 0.34 -0.0273 Manganese 0.46 0.0273 0.34 0.0172 0.44 0.0131 0.34 0.0137 0.34 0.00683 Molybdenum 0.46 0.0273 0.3 -0.0068 0.4 -0.00437 0.34 0.0171 0.34 0.030 Nickel 0.91 0.0365 0.69 0.0344 0.87 0.0218 0.68 0.431 0.68 0.023 Selenium 0.91 -0.210 0.69 0.117 0.8 -0.131 0.68 0.0308 0.68 0.0376 Silver 0.91 -0.00456 0.6q 0.0q 0.87 0.00 0.68 0.00684 0.68 0.047 Thallium 0.91 -0.278 0.6 -0.145 0.8 -0.122 0.68 -0.154 0.68 -0.143 Vanadium 0.46 0.00456 0.34 0.0276 0.4 -0.00437 0.34 0.0200 0.34 0.013 Zinc 0.91 0.0775 0.69 0.0689 0.871 0.0611 0.68 0.0615 0.68 -0.020 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 4 of 4 Page 25 Of 32 OrderID: 332404002 I., w v � C C C C C C C C C C n n n n n n n n n n n n>> n n n n> n -c a 0 w 0 w 0 w 0 w O w o w 0 w a w a w a w s a rt (� cl , fD O K m 0 m 0 m 0 rn 0 m 0 m 0 m 0 m 0 m 0 m a rCo D m * n 0 n 0 n 0 0 0 0 0 0 0 �, o n > n n n n n v 0 FL 7 in rD m O m O m C] m O m O m Q rn O m O m O rn 0 w n x w n n n n n n n o � rD � Lm rt r s e a ;Q, G s, w cu t� W iN w wkA 3 ro rD CA 0 v ED ro rDLn V1 Vt •— ._ N .� Cl� .� c s 1 .� w Ui U� . [ _ . C l h 0 a 3 s � a .c cJ'� m ry H X X X X X X X X X X CAM 16 + Al and Mn rD _ S 0 a n n n n n n D n n it � II II n Page 26 Of 32 x Paae 1 Of 3 m rrD rn 7 f0 0 u, cr+ n 3 p a m o3 o c o N oo P7 n Cn 0 rD rD O 3 n 0 ° Q 3 ro z 0 r m =ptA W p ❑ � !� CD d c rlm 3 0 0 d x m m W' ❑ o m m� 3 6 c o . O rD Q- - "�'� .� O. n Cr m N fG m # X .Xi 2 rD :r m c 'M c m ° a "o m a '° " a : -.0 a O m 3 fD �� ❑ w N � n N = t0 O N cl at I - 3 Q H d l�D m rp ❑ rD < x• rp c^ cu ❑■ ❑ a 0 13 x m cn C7 Z a rn r �J OrderID: 332404002 w -� n c c c c c c c c e n 2 m n n n n n n n n n > Ln n n n > n n n > n 0 of z 0 0 0 0 0 0 a 0 w 3 p �0 Q m O 3 _ K m O_ m p m 0 m 0 m 0 m 0 m 0 m 0 rrn 0 m 0 m 0 T 00 aa) 0 0 0 0 0 0 0 0 0 0 O co < lD w -! a) U9 � w N F-+ 0 n' 3 CD co w m m a, w m m n v 0 O m Q m7 (.n rD n D m o m 0 m 0 m 0 m 0 m 0 m 0 m 0 m 0 -na' w c 3 0 m 0 0 0 0 0 0 0 0 0 0 n Q W Z ED 00 w V co a1 m Ln co ? co w w N wcc; i 0 a7 n m W cam- N o Ep U1 au cxlt om 0 rn r r r r r r r r r r O d^ m p L 70 0 LA 03 m n r � N N .G o$C? N .� OQ 3 rfl -t m � m $ a w a�i p a_ lu r m Nr .c m e s s s s L4 �� WC CAW N � W ,� �� N � a Sv goo N 'J X- o� Lh 3 ro U O L X X X X X X X X X X CAM 16+Aland Mn m _ Z � m S O Q n n n n n n n > n n Paqe 27 Of 32 Paqe 2 Of 3 :1 o �fl-�3 a ro Ln 0 co O F-� 00 0 0 3 v o m o ❑ c r0 3 a 3 s o m a O 0 0 a 0 a 3 rn o m M Z Q # Ufa X ro z a r-Eb r- r-D a � �. H ro rD a o >a ,* a a O D In ■� ❑ w NLnn ro Z N = Q n 3 �O o d 0 3 41 a (D ro ElfD m C 77 t9 Ln w ON = 3 ro ❑ 0 cu S [1D ❑ 0 C 0 0 z z r.. m jo m T 0 no 4u CA CN IV 3 OrderID: 332404002 1n O L) U e n 0 w w lu f) Ccu r) C r- C) D cu ai z W O 3 :z o 0 _ m r( 3 m p m av m o O w + r. co o o �, n < r-■ m nn, a© r* 0 3 0 D cn n � m i o =� 3 =0 ® m O Q 1--' n "0 1Z co Ep O C m m . C con L, cu d h m c n m r r 3 C m Ln Ln 0 r+ 3 0� CD f° w -SIX c� q� m 1n ti m 3 -� L v CU e •e -� 3 W 3 �F CAM 16 + Al X X and Mn m ' - z r 0 a a ro g x h Paqe 28 Of 32 " Paqe 3 Of 3 0 =s rn o �- --I 4-1 N K7 O = 00 z ` n 00 Ul O N O O m 0 z 0 r ro z 0 n LA D x LA m LA N 0~0 D ,v n O 3 ° ❑ :v � =�m�Qo os 7 C1 S O rt ro O_ a m X rD fD O h� N � A " " c. `�° `T. rt [, t+ '' .. o rD fD � D ❑ z w oQ to 0 �W�Qj a CL ro m N ❑� = m 3 �o ❑ Q O r, z m z m 0 r n n_ Z 0 C) C CA 4 o44 vw W zN v� n� z �- r � V'1 r,-3 m /on m 0 X ., LA Testing 5431 Industrial Drive, Huntington Beach, CA 92649 /Pir Phone: (714) 828-4999 Fax: (714) 828-4944 I Email: hblab@latesting.com TESTING Attn: Noah Ambos Customer ID: CTEH99 CTEH Center for Toxicology & Env. Health Customer PO: 5120 North Shore Drive Received: 03/07/24 9:25 AM North Little Rock, AR 72118 Fax: (501) 614-2835 Phone: (501) 454-1622 LA Testing Order: 332404002 Project: PRO7-032229 LA Testing Proj ID: PROJ-032229 Cust COC ID Project Type: Standard Project Receipt Confirmation Shipping Tracking Number: EMSL Received Cust Sample Order ID Test Date TAT Due Date TUCA0306ME001A 332404002-0001 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME001A 332404002-0001 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME002A 332404002-0002 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME002A 332404002-0002 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME003A 332404002-0003 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME003A 332404002-0003 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME004A 332404002-0004 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME004A 332404002-0004 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME005A 332404002-0005 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME005A 332404002-0005 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME006A 332404002-0006 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME006A 332404002-0006 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME007A 332404002-0007 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM Date Sent 31712024 9:38:11 AM Paqe 29 Of 32 1 911ALA Testing 5431 Industrial Drive, Huntington Beach, CA 92649 Phone: (714) 828-4999 Fax: (714) 828-4944 Email: hblab@latesting.com TESTING Attn: Noah Ambos Customer ID: CTEH99 CTEH Center for Toxicology & Env. Health Customer PO: 5120 North Shore Drive Received: 03/07/24 9:25 AM North Little Rock, AR 72118 Fax: (501) 614-2835 Phone: (501) 454-1622 LA Testing Order: 332404002 Project: PRO7-032229 LA Testing Proj ID: PROJ-032229 Cust COC ID Project Type: Standard Project Receipt Confirmation Shipping Tracking Number: EMSL Received Cust Sample Order ID Test Date TAT Due Date TUCA0306ME007A 332404002-0007 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME008A 332404002-0008 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME008A 332404002-0008 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME009A 332404002-0009 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME009A 332404002-0009 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME010A 332404002-0010 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME010A 332404002-0010 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306MEFBO01A 332404002-0011 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306MEFBO01A 332404002-0011 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME001B 332404002-0012 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME001B 332404002-0012 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME002B 332404002-0013 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME002B 332404002-0013 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM Date Sent 31712024 9:38:11 AM Paqe 30 Of 32 2 911ALA Testing 5431 Industrial Drive, Huntington Beach, CA 92649 Phone: (714) 828-4999 Fax: (714) 828-4944 Email: hblab@latesting.com TESTING Attn: Noah Ambos Customer ID: CTEH99 CTEH Center for Toxicology & Env. Health Customer PO: 5120 North Shore Drive Received: 03/07/24 9:25 AM North Little Rock, AR 72118 Fax: (501) 614-2835 Phone: (501) 454-1622 LA Testing Order: 332404002 Project: PRO7-032229 LA Testing Proj ID: PROJ-032229 Cust COC ID Project Type: Standard Project Receipt Confirmation Shipping Tracking Number: EMSL Received Cust Sample Order ID Test Date TAT Due Date TUCA0306ME003B 332404002-0014 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME003B 332404002-0014 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME004B 332404002-0015 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME004B 332404002-0015 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME005B 332404002-0016 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME005B 332404002-0016 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME006B 332404002-0017 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME006B 332404002-0017 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME007B 332404002-0018 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME007B 332404002-0018 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME008B 332404002-0019 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME008B 332404002-0019 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME009B 332404002-0020 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM Date Sent 31712024 9:38:11 AM Paqe 31 Of 32 3 911ALA Testing 5431 Industrial Drive, Huntington Beach, CA 92649 Phone: (714) 828-4999 Fax: (714) 828-4944 Email: hblab@latesting.com TESTING Attn: Noah Ambos Customer ID: CTEH99 CTEH Center for Toxicology & Env. Health Customer PO: 5120 North Shore Drive Received: 03/07/24 9:25 AM North Little Rock, AR 72118 Fax: (501) 614-2835 Phone: (501) 454-1622 LA Testing Order: 332404002 Project: PRO7-032229 LA Testing Proj ID: PROJ-032229 Cust COC ID Project Type: Standard Project Receipt Confirmation Shipping Tracking Number: EMSL Received Cust Sample Order ID Test Date TAT Due Date TUCA0306ME009B 332404002-0020 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME010B 332404002-0021 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306ME010B 332404002-0021 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306MEFBO01B 332404002-0022 C-CAM 16 Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM TUCA0306MEFBO01B 332404002-0022 C-Metals by ICP 3/7/2024 1 Week (EOD) 3/14/2024 9:25:00 AM 6:00:00 PM Note: The above sample log -in information is based solely on the data provided by the customer on the Chain of Custody form. Sample count, ID number verification, and evaluation of each individual sample is not started/done until sample analysis process begins by the scientist at the lab bench. If at this point the staff finds that a sample is missing, ID number does not match, or has any other issue that will disrupt analysis, the customer will be notified. Date Sent 31712024 9:38:11 AM Paqe 32 Of 32 4