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HomeMy WebLinkAboutMetals 03172024LA TESTING g.'A TESTING Noah Ambos CTEH Center for Toxicology & Env. Health 5120 North Shore Drive North Little Rock, AR 72118 LA Testing 5431 Industrial Drive Huntington Beach, CA 92649 (714) 828-4999 CustomerService(o)emsl.com Re: Narrative: NIOSH 7303 LA Testing Order: 332404852, Project ID: PROJ-032229 Dear Noah HUNTINGTON BEACH, CA 92649 5431 INDUSTRIAL DRIVE PHONE: (714) 828-4999 On 3/18/2024, LA Testing Huntington Beach, CA received 22 air samples for metals analysis via NIOSH 7300 Modified method. The samples were received and logged in following normal lab procedures. All samples were received under Chain of Custody and in good condition unless otherwise noted. NIOSH 7300 Modified LA Testing Order: 332404852, Project ID: PROJ-032229: All samples were prepared and analyzed according to the method specified NIOSH 7300 Modified. The samples were submitted on cellulose ester membrane filters which were prepared utilizing a hot block digestion technique as indicated in the method. The samples were then analyzed via Inductively Coupled Plasma (ICP) analysis utilizing Atomic Emission Spectroscopy (AES). All preparation and analyses were performed within the method specific hold time requirement. Results are reported in mg/m3. Quality Control Dilutions: None Calibrations: The RL, RLVS ICV and bracketing CCV standards were within control limits. Blanks: Target analytes were not detected above the reporting limit in the associated blanks. Media blank was not subtracted from sample concentrations. LCS/LCSD: The laboratory control sample spike recoveries and RPD results were within control limits. ICSA/ICSB: The interference check solution results were within control limits. QC was performed at rates compliant with both the American Industrial Hygiene Association (AIHA) and the California Environmental Laboratory Accreditation Program (ELAP). 1 certify that this report is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. In addition, I certify, that to the best of my knowledge and belief, the data as reported are true and accurate. Release of the data contained in this Michael Chapman, Laboratory Manager q• Paqe 1 Of March 25, 2024 CHEMMETALNARR.2.0 LA Testing 5431 Industrial Drive, Huntington Beach, CA 92649 Phone: (714) 828-4999 Fax: (714) 828-4944 Email: hblabOlatestinq.com TESTING Attn: Noah Ambos 3/25/2024 CTEH Center for Toxicology & Env. Health 5120 North Shore Drive North Little Rock, AR 72118 Phone: (501) 801-8500 Fax: (501) 614-2835 The following analytical report covers the analysis performed on samples submitted to LA Testing on 3/18/2024. The results are tabulated on the attached data pages for the following client designated project: Project ID: PROJ-032229 PROJ-032229 The reference number for these samples is EMSL Order #332404852. Please use this reference when calling about these samples. If you have any questions, please do not hesitate to contact me at (714) 828-4999. Approved By: Michael Chapman, Laboratory Manager AIHA LAP, LLC-IHLAP Accredited #101650 EMSL maintains liability limited to cost of analysis. Interpretation and use of test results are the responsibility of the client. This report relates only to the samples reported above, and may not be reproduced, except in full, without written approval by EMSL. EMSL bears no responsibility for sample collection activities or analytical method limitations. The report reflects the samples as received. Results are generated from the field sampling data (sampling volumes and areas, locations, etc.) provided by the client on the Chain of Custody. Samples are within quality control criteria and met method specifications unless otherwise noted. Page 1 of 16 Paqe 2 Of 30 LA Testing LA Testing Order: 332404852 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/18/2024 10:45 AM North Little Rock, AR 72118 Collected: 3/17/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0317ME001A Collected. 3/17/2024 Lab ID: 332404852-0001 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.071 0.071 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Molybdenum <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH Client Sample Description TUCA0317ME002A Collected. 3/17/2024 Lab ID: 332404852-0002 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.071 0.071 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/25/2024 5:36:45 PM Page 2 of 16 Paqe 3 Of 30 LA Testing LA Testing Order: 332404852 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/18/2024 10:45 AM North Little Rock, AR 72118 Collected: 3/17/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0317ME002A Collected. 3/17/2024 Lab ID: 332404852-0002 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH Client Sample Description TUCA0317ME003A Collected. 3/17/2024 Lab ID: 332404852-0003 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.073 0.073 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.15 0.15 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Molybdenum <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/25/2024 5:36:45 PM Page 3 of 16 Paqe 4 Of 30 LA Testing LA Testing Order: 332404852 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/18/2024 10:45 AM North Little Rock, AR 72118 Collected: 3/17/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0317ME004A Collected. 3/17/2024 Lab ID: 332404852-0004 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.071 0.071 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH Client Sample Description TUCA0317ME005A Collected. 3/17/2024 Lab ID: 332404852-0005 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.072 0.072 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/25/2024 5:36:45 PM Page 4 of 16 Paqe 5 Of 30 LA Testing LA Testing Order: 332404852 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/18/2024 10:45 AM North Little Rock, AR 72118 Collected: 3/17/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0317ME005A Collected. 3/17/2024 Lab ID: 332404852-0005 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH Client Sample Description TUCA0317ME006A Collected. 3/17/2024 Lab ID: 332404852-0006 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.073 0.073 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.15 0.15 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Molybdenum <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.73 0.73 pg/m' 3/21/2024 XL 3/22/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/25/2024 5:36:45 PM Page 5 of 16 Paqe 6 Of 30 LA Testing LA Testing Order: 332404852 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/18/2024 10:45 AM North Little Rock, AR 72118 Collected: 3/17/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0317ME007A Collected. 3/17/2024 Lab ID: 332404852-0007 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.071 0.071 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Molybdenum <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH Client Sample Description TUCA0317ME008A Collected. 3/17/2024 Lab ID: 332404852-0008 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.071 0.071 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/25/2024 5:36:45 PM Page 6 of 16 Paqe 7 Of 30 LA Testing LA Testing Order: 332404852 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/18/2024 10:45 AM North Little Rock, AR 72118 Collected: 3/17/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0317ME008A Collected. 3/17/2024 Lab ID: 332404852-0008 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH Client Sample Description TUCA0317ME009A Collected. 3/17/2024 Lab ID: 332404852-0009 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <5.5 5.5 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <1.1 1.1 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <1.1 1.1 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <5.5 5.5 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.11 0.11 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.22 0.22 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <1.1 1.1 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.55 0.55 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <1.1 1.1 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.55 0.55 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.55 0.55 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Molybdenum <0.55 0.55 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <1.1 1.1 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <1.1 1.1 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <1.1 1.1 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <1.1 1.1 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.55 0.55 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <1.1 1.1 pg/m' 3/21/2024 XL 3/22/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/25/2024 5:36:45 PM Page 7 of 16 Paqe 8 Of 30 LA Testing LA Testing Order: 332404852 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/18/2024 10:45 AM North Little Rock, AR 72118 Collected: 3/17/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0317ME010A Collected. 3/17/2024 Lab ID: 332404852-0010 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.6 3.6 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.072 0.072 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Molybdenum <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.36 0.36 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.72 0.72 pg/m' 3/21/2024 XL 3/22/2024 TH Client Sample Description TUCA0317MEFBO01A Collected. 3/17/2024 Lab ID: 332404852-0011 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <5.0 5.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <5.0 5.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.10 0.10 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.20 0.20 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.50 0.50 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.50 0.50 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.50 0.50 pg/filter 3/21/2024 XL 3/22/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/25/2024 5:36:45 PM Page 8 of 16 Paqe 9 Of 30 LA Testing LA Testing Order: 332404852 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/18/2024 10:45 AM North Little Rock, AR 72118 Collected: 3/17/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0317MEFBO01A Collected. 3/17/2024 Lab ID: 332404852-0011 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.50 0.50 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.50 0.50 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH Client Sample Description TUCA0317ME001 B Collected. 3/17/2024 Lab ID: 332404852-0012 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.4 3.4 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.4 3.4 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.068 0.068 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.34 0.34 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.34 0.34 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.34 0.34 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Molybdenum <0.34 0.34 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.34 0.34 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/25/2024 5:36:45 PM Page 9 of 16 Paqe 10 Of 30 LA Testing LA Testing Order: 332404852 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/18/2024 10:45 AM North Little Rock, AR 72118 Collected: 3/17/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0317ME002B Collected. 3/17/2024 Lab ID: 332404852-0013 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.4 3.4 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.4 3.4 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.068 0.068 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.34 0.34 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.34 0.34 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.34 0.34 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Molybdenum <0.34 0.34 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.34 0.34 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH Client Sample Description TUCA0317ME003B Collected. 3/17/2024 Lab ID: 332404852-0014 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.4 3.4 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.4 3.4 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.068 0.068 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.34 0.34 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.34 0.34 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.34 0.34 pg/m' 3/21/2024 XL 3/22/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/25/2024 5:36:45 PM Page 10 of 16 Paqe 11 Of 30 LA Testing LA Testing Order: 332404852 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/18/2024 10:45 AM North Little Rock, AR 72118 Collected: 3/17/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0317ME003B Collected. 3/17/2024 Lab ID: 332404852-0014 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.34 0.34 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.34 0.34 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.68 0.68 pg/m' 3/21/2024 XL 3/22/2024 TH Client Sample Description TUCA0317ME004B Collected. 3/17/2024 Lab ID: 332404852-0015 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.69 0.69 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.69 0.69 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.069 0.069 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.69 0.69 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.69 0.69 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.69 0.69 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.69 0.69 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.69 0.69 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.69 0.69 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.69 0.69 pg/m' 3/21/2024 XL 3/22/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/25/2024 5:36:45 PM Page 11 of 16 Paqe 12 Of 30 LA Testing LA Testing Order: 332404852 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/18/2024 10:45 AM North Little Rock, AR 72118 Collected: 3/17/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0317ME005B Collected. 3/17/2024 Lab ID: 332404852-0016 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.70 0.70 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.70 0.70 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.070 0.070 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.70 0.70 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.70 0.70 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.70 0.70 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.70 0.70 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.70 0.70 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.70 0.70 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.70 0.70 pg/m' 3/21/2024 XL 3/22/2024 TH Client Sample Description TUCA0317ME006B Collected. 3/17/2024 Lab ID: 332404852-0017 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <5.2 5.2 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <1.0 1.0 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <1.0 1.0 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <5.2 5.2 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.10 0.10 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.21 0.21 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <1.0 1.0 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.52 0.52 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <1.0 1.0 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.52 0.52 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.52 0.52 pg/m' 3/21/2024 XL 3/22/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/25/2024 5:36:45 PM Page 12 of 16 Paqe 13 Of 30 LA Testing LA Testing Order: 332404852 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/18/2024 10:45 AM North Little Rock, AR 72118 Collected: 3/17/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0317ME006B Collected. 3/17/2024 Lab ID: 332404852-0017 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.52 0.52 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <1.0 1.0 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <1.0 1.0 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <1.0 1.0 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <1.0 1.0 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.52 0.52 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <1.0 1.0 pg/m' 3/21/2024 XL 3/22/2024 TH Client Sample Description TUCA0317ME007B Collected. 3/17/2024 Lab ID: 332404852-0018 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <4.8 4.8 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.95 0.95 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.95 0.95 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <4.8 4.8 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.095 0.095 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.19 0.19 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.95 0.95 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.48 0.48 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.95 0.95 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.48 0.48 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.48 0.48 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Molybdenum <0.48 0.48 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.95 0.95 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.95 0.95 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.95 0.95 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.95 0.95 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.48 0.48 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.95 0.95 pg/m' 3/21/2024 XL 3/22/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/25/2024 5:36:45 PM Page 13 of 16 Paqe 14 Of 30 LA Testing LA Testing Order: 332404852 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/18/2024 10:45 AM North Little Rock, AR 72118 Collected: 3/17/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0317ME008B Collected. 3/17/2024 Lab ID: 332404852-0019 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.071 0.071 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH Client Sample Description TUCA0317ME009B Collected. 3/17/2024 Lab ID: 332404852-0020 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.071 0.071 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/25/2024 5:36:45 PM Page 14 of 16 Paqe 15 Of 30 LA Testing LA Testing Order: 332404852 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/18/2024 10:45 AM North Little Rock, AR 72118 Collected: 3/17/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0317ME009B Collected. 3/17/2024 Lab ID: 332404852-0020 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH Client Sample Description TUCA0317ME010B Collected. 3/17/2024 Lab ID: 332404852-0021 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.071 0.071 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <0.71 0.71 pg/m' 3/21/2024 XL 3/22/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/25/2024 5:36:45 PM Page 15 of 16 Paqe 16 Of 30 LA Testing LA Testing Order: 332404852 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/18/2024 10:45 AM North Little Rock, AR 72118 Collected: 3/17/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0317MEFBO01 B Collected. 3/17/2024 Lab ID: 332404852-0022 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <5.0 5.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Antimony <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Arsenic <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Barium <5.0 5.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Beryllium <0.10 0.10 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Cadmium <0.20 0.20 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Chromium <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Cobalt <0.50 0.50 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Copper <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Lead <0.50 0.50 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Manganese <0.50 0.50 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Molybdenum <0.50 0.50 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Nickel <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Selenium <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Silver <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Thallium <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Vanadium <0.50 0.50 pg/filter 3/21/2024 XL 3/22/2024 TH 7300 Modified Zinc <1.0 1.0 pg/filter 3/21/2024 XL 3/22/2024 TH AIHA LAP, LLC-IHLAP Accredited #101650 Definitions: MDL - method detection limit J - Result was below the reporting limit, but at or above the MDL ND - indicates that the analyte was not detected at the reporting limit RL - Reporting Limit (Analytical) D - Dilution Sample required a dilution which was used to calculate final results ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 3/25/2024 5:36:45 PM Page 16 of 16 Paqe 17 Of 30 Printed: 3/25/2024 Batch: 33Q240321-3MCE Instrument: 33-PE8300 Initial Cal Std: Cal Check Std: Internal Std: LCS Std MS Std Matrix: Cassettes ICP QC Batch Summary Created: 3/21/24 2:03 pm By: xle 332404852-0001 332404852-0005 332404852-0009 332404852-0013 332404852-0017 332404852-0002 332404852-0006 332404852-0010 332404852-0014 332404852-0018 332404852-0003 332404852-0007 332404852-0011 332404852-0015 332404852-0019 332404852-0004 332404852-0008 332404852-0012 332404852-0016 332404852-0020 Blank/DL Control Other Matrix Blank[7] Method Blank[7] LCSD[7] LCS[1] 332404852-0001 03/22/24 09:31 03/22/24 09:34 03/22/24 09:42 03/22/24 09:44 03/22/24 12:34 Result pg/filter RL pg/filter IL Result pg/filter RL pgKiilter Result pg/filter True Conc pg/filter % Rec 73.7051-119. 552 % RPD <=20 Result pg/filter True Conc pg/filter % Rec 73.7051-119. 552 RL pg/m3 Result pg/m' Aluminum -0.64 5. -1.22 5.0 22.7 25.0 90.7 1.20 22.4 25.0 89.6 3. -0.071 Antimony 0.075 1. -0.280 1.0 24.0 25.0 95.9 1.96 23.5 25.0 94.1 0.71 -0.20 Arsenic -0.40 1. -0.280, 1.0 23.9 25.0 95.4 5.14 22.7 25.0 90.6 0.71 -0.20 Barium 0.0 5. 0.0450 5.0 23.8 25. 95.3 0.0839 23.8 25.0 95.3 3.6 0.032 Beryllium 0.0050 0.1 0.010 0.1 23.9 25. 95.5 0.147 23.9 25.0 95.6 0.071 0.0 Cadmium 0.015 0.2 0.010 0.2 25.4 25. 102 1.41 25.1 25.0 100 0.14 0.0071 Chromium -0.015 1. -0.040 1. 23.9 25. 95.6 0.462 23.8 25.0 95.1 0.71 0.028 Cobalt 0.0300 0.50 0.21 0.5 26.1 25.0 105 1.72 25.7 25.0 103 0.36 0.021 Copper 0.00 1.0 0.55 1. 24.7 25. 98. 0.203 24.6 25.0 98.5 0.71 0.16 Lead -0.0100 0.50 0.0650 0.50 24.2 25. 96.9 0.642 24.1 25.0 96.3 0.3 -0.092 Manganese 0.00 0.5 -0.0200 0.50 25.0 25. 100 0.280 24.9 25.0 99.7 0.36 0.024 Molybdenum 0.0100 0.50 0.275 0.50 25.9 25.0 104 1.09 25.6 25.0 102 0.3 -0.017 Nickel 0.0300 1.0 0.0150 1.0 26.3 25. 105 1.98 25.8 25.0 103 0.71 0.035 Selenium 0.185 1.0 0.240 1.0 23.9 25. 95.5 1.54 23.5 25.0 94.1 0.71 0.021 Silver 0.0300 1.0 0.15q 1.q 23.4 25. 93.71 0.426 23.5 25.0 94.11 0.71 0.024 Thallium 0.0200 1.0 0.135 1. 25.2 25. 101 1.20 24.9 25.0 99.6 0.71 0.20 Vanadium 0.0200 0.5 -1.00 0.5 24.4 25. 97.5 0.370 24.3 25.0 97.1 0.3 -0.024 Zinc -0.040 1. -0.110 1. 26.q 25. 104 1.69 25.6 25.0 102 0.71 0.13 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 1 of 4 Page 18 Of 30 Printed: 3/25/2024 ICP QC Batch Summary Batch: 33Q240321-3MCE Created: 3/21/24 2:03 pm By: xle Instrument: 33-PE8300 Initial Cal Std: Samples: Cal Check Std: Internal Std: 332404852-0001 332404852-0005 332404852-0009 LCS Std 332404852-0002 332404852-0006 332404852-0010 332404852-0003 332404852-0007 332404852-0011 MS Std Matrix: Cassettes 332404852-0004 332404852-0008 332404852-0012 332404852-0013 332404852-0017 332404852-0014 332404852-0018 332404852-0015 332404852-0019 332404852-0016 332404852-0020 Other 332404852-0002 332404852-0003 332404852-0004 332404852-0005 332404852-0007 332404852-0008 332404852-0009 03/22/2412:36 03/22/2412:43 03/22/2412:45 03/22/2412:48 03/22/2412:52 03/22/2412:55 03/22/2412:57 RL pg/m' Result Ng/m3 RL pg/m' Result Ng/m' RL pg/m' Result Ng/m' RL pg/m' Result pg/m' RL pg/m' Result Ng/m' RL pg/m' Result pg/m' RL pg/m' Result Ng/m3 Aluminum 3. -0.0285 3.6 0.127 3.5 0.53 3.6 0.0537 3.6 0.00 3.6 0.182 5. -0.231 Antimony 0.71 -0.067 0.7 -0.192 0.71 -0.010 0.72 -0.0572 0.71 -0.268 0.71 -0.411 1.1 -0.099 Arsenic 0.71 -0.0997 0.7 -0.283 0.71 -0.43 0.72 -0.279 0.71 -0.0893 0.71 -0.47 1.1 -0.24 Barium 3.6 0.0285 3.6 0.0290 3.5 0.0354 3.6 0.0286 3.6 0.0250 3.6 0.0321 5.5 0.038 Beryllium 0.071 0.00356 0.073 0.00 0.071 0.00354 0.072 0.00 0.071 0.00 0.071 0.00357 0.11 0.0 Cadmium 0.14 0.0107 0.15 0.0109 0.14 0.00709 0.14 0.0143 0.14 0.0107 0.14 0.00357 0.22 0.00551 Chromium 0.71 0.0249 0.73 0.0436 0.71 0.181 0.72 0.182 0.71 0.0250 0.71 0.0286 1.1 0.22 Cobalt 0.36 0.0249 0.36 0.0181 0.3 -0.00709 0.36 0.0071 0.36 -0.00714 0.36 0.0143 0.5 -0.027 Copper 0.71 0.142 0.7q 0.232 0.71 0.188 0.72 0.179 0.71 0.146 0.71 0.143 1.1 0.23 Lead 0.3 -0.092 0.3 -0.069 0.3 -0.0921 0.36 -0.143 0.36 -0.0536 0.3 -0.085 0.5 -0.33 Manganese 0.36 0.0142 0.36 0.0218 0.35 0.0142 0.36 0.0107 0.36 0.0143 0.36 0.0143 0.55 0.022 Molybdenum 0.36 0.0107 0.36 0.00726 0.35 0.0248 0.36 -0.0250 0.36 0.00714 0.36 0.00357 0.55 0.0 Nickel 0.71 0.0249 0.73 0.0363 0.71 0.0425 0.72 0.0286 0.71 0.0321 0.71 0.0429 1.1 0.027 Selenium 0.71 0.110 0.73 0.290 0.71 0.0354 0.72 0.258 0.71 0.0214 0.71 0.00357 1.1 0.45 Silver 0.71 0.0142 0.7q 0.0251 0.71 0.0319 0.72 0.0179 0.71 0.0286 0.71 0.0107 1.1 0.0441 Thallium 0.71 0.221 0.7 0.032 0.71 -0.00354 0.72 0.00 0.71 0.12q 0.711 0.118 1.11 0.121 Vanadium 0.3 -0.00356 0.3 0.0036 0.3 -0.010 0.36 -0.00715 0.36 0.00 0.3 -0.0035 0.5 -0.038 Zinc 0.71 0.0641 0.7 0.160 0.711 0.110 0.72 0.0859 0.71 0.104 0.711 0.129 1.11 0.14 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 2 of 4 Page 19 Of 30 Printed: 3/25/2024 ICP QC Batch Summary Batch: 33Q240321-3MCE Created: 3/21/24 2:03 pm By: xle Instrument: 33-PE8300 Initial Cal Std: Samples: Cal Check Std: Internal Std: 332404852-0001 332404852-0005 332404852-0009 LCS Std 332404852-0002 332404852-0006 332404852-0010 332404852-0003 332404852-0007 332404852-0011 MS Std Matrix: Cassettes 332404852-0004 332404852-0008 332404852-0012 332404852-0013 332404852-0017 332404852-0014 332404852-0018 332404852-0015 332404852-0019 332404852-0016 332404852-0020 Other 332404852-0010 332404852-0011 332404852-0012 332404852-0014 332404852-0015 332404852-0016 332404852-0017 03/22/2412:59 03/22/2413:02 03/22/2413:04 03/22/2413:13 03/22/2413:16 03/22/2413:18 03/22/2413:20 RL pg/m' Result Ng/m' RL pg/filter Result pg/filter RL pg/m' Result Ng/m' RL pg/m' Result pg/m' RL pg/m' Result Ng/m' RL pg/m' Result pg/m' RL pg/m' Result pg/m' Aluminum 3. -0.187 5.0 0.0050C 3.4 0.298 3.4 -0.0514 3.5 0.0451 3. -0.0696 5.2 0.12 Antimony 0.72 -0.241 1.0 0.21C 0.68 0.328 0.68 -0.0548 0.69 0.440 0.70 -0.522 1.0 0.53 Arsenic 0.7 -0.093 1. -0.065 0.6 -0.0137 0.68 0.0787 0.69 -0.142 0.70, 0.146 1. -0.24 Barium 3.6 0.0323 5.0 0.030C 3.4 0.0445 3.4 0.0240 3.5 0.0312 3.5 0.0244 5.2 0.031 Beryllium 0.072 0.00 0.10 0.00500 0.068 0.00342 0.068 0.00 0.069 0.00 0.070 0.00, 0.10 0.0052 Cadmium 0.14 0.00359 0.20 0.0100 0.14 0.00684 0.14 0.00342 0.14 0.00693 0.14 0.0104 0.21 0.015 Chromium 0.72 0.0216 1.0 0.245 0.68 0.192 0.68 0.0171 0.69 0.0243 0.70 0.184 1.0 0.042 Cobalt 0.36 0.00359 0.50 0.0100 0.34 0.00684 0.34 0.0171 0.35 0.0208 0.35 0.0104 0.52 0.021 Copper 0.72 0.154 1.q 0.195 0.68 0.150 0.6q 0.154 0.69 0.156 0.70 0.157 1.0 0.19 Lead 0.3 -0.12 0.5 -0.205 0.34 0.0445 0.3 -0.171 0.3 -0.0901 0.3 -0.0591 0.5 -0.073 Manganese 0.36 0.021 0.5 0.0100 0.34 0.0308 0.34 0.0137 0.35 0.0139 0.35 0.0104 0.52 0.026 Molybdenum 0.36 0.0251 0.5 0.0100 0.3 -0.013 0.34 -0.0171 0.35 0.0208 0.3 -0.0034 0.5 -0.010 Nickel 0.72 0.028 1. 0.0550 0.68 0.0410 0.68 0.0274 0.69 0.0208 0.70 0.0313 1.0 0.047 Selenium 0.72 0.55 1. 0.275 0.68 0.414 0.68 0.312 0.69 0.378 0.70 0.191 1.0 0.60 Silver 0.72 0.0251 1.q 0.040q 0.6 -0.00684 0.68 0.0171 0.69 0.0243 0.70 0.00348 1.0 0.052 Thallium 0.72 0.108 1. 0.18 0.68 0.0855 0.68 0.106 0.69 0.00693 0.70 -0.0174 1.q 0.094 Vanadium 0.3 -0.014 0.5 -0.015 0.3 -0.00342 0.34 0.0137 0.3 -0.013 0.3 -0.0104 0.521 0.031 Zinc 0.721 0.0970 1. 0.12 0.6q 0.133 0.68 0.0616 0.69 0.0936 0.70 0.0696 1.0 0.131 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 3 of 4 Page 20 Of 30 Printed: 3/25/2024 Batch: 33Q240321-3 M C E Instrument: 33-PE8300 Initial Cal Std: Cal Check Std: Internal Std: LCS Std MS Std Matrix: Cassettes ICP QC Batch Summary Created: 3/21/24 2:03 pm By: xle Samples: 332404852-0001 332404852-0002 332404852-0003 332404852-0004 332404852-0005 332404852-0009 332404852-0006 332404852-0010 332404852-0007 332404852-0011 332404852-0008 332404852-0012 332404852-0013 332404852-0017 332404852-0014 332404852-0018 332404852-0015 332404852-0019 332404852-0016 332404852-0020 Other 332404852-0018 332404852-0019 332404852-0020 332404852-0006 332404852-0013 03/22/2413:23 03/22/2413:25 03/22/2413:27 03/22/2414:23 03/22/2414:25 RL pg/m3 Result pg/m' RL pg/m' Result pg/m' RL pg/m' Result pg/m; RL pg/m' Result pg/m' RL pg/m' Result pg/m' Aluminum 4. -0.21 3. -0.070 3. -0.0247 3.6 0.0546 3.4 -0.123 Antimony 0.9 -0.109 0.71 -0.088 0.71 -0.370 0.73 0.233 0.68 0.322 Arsenic 0.9 -0.0238 0.71 -0.279 0.71 -0.395 0.73 -0.142 0.68 0.0718 Barium 4.8 0.0333 3.5 0.0318 3.5 0.0282 3.6 0.0291 3.4 0.023 Beryllium 0.095 0.00475 0.071 0.00 0.071 0.00 0.073 0.00364 0.068 0.00342 Cadmium 0.19 0.0143 0.14 0.0106 0.14 0.00353 0.15 0.0182 0.14 0.00684 Chromium 0.95 0.0618 0.71 0.0141 0.71 0.0388 0.73 0.0255 0.68 0.013 Cobalt 0.48 0.0285 0.35 0.0177 0.3 -0.0035 0.3 -0.010 0.34 -0.0137 Copper 0.95 0.238 0.711 0.141 0.71 0.145 0.73 0.146 0.68 0.120 Lead 0.4 -0.105 0.3 -0.095 0.3 -0.024 0.36 -0.124 0.34 -0.0547 Manganese 0.48 0.0285 0.35 0.0212 0.35 0.0176 0.36 0.0146 0.34 0.013 Molybdenum 0.4 -0.00475 0.35 0.0106 0.3 -0.0070 0.36 -0.025 0.34 -0.0308 Nickel 0.95 0.0428 0.71 0.0283 0.71 0.0388 0.73 0.0218 0.68 0.0376 Selenium 0.95 0.166 0.71 0.212 0.71 0.448 0.73 0.135 0.68 0.274 Silver 0.95 0.0523 0.71 0.00354 0.71 0.00353 0.73 0.0437 0.68 0.0342 Thallium 0.95 0.152 0.71 -0.0495 0.71 0.0212 0.73 0.0910 0.68 0.085 Vanadium 0.4 -0.0285 0.35 0.00 0.35 0.0212 0.36 -0.00364 0.34 0.030 Zinc O.gq 0.105 0.71 0.0884 0.711 0.0882 0.73 0.0838 0.68 0.085 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 4 of 4 Page 21 Of 30 Printed Batch: Instrument: Initial Cal Std: Cal Check Std: Internal Std: LCS Std MS Std Matrix: 3/25/2024 33Q240321-6MCE 33-PE8300 Cassettes I ICP QC Batch Summary Created: 3/21/24 2:09 pm By: xle 332404846-0021 332404982-0021 332404846-0022 332404982-0022 332404852-0021 332404987-0021 332404852-0022 332404987-0022 Blank/DL Control Other Method Blank[7] Matrix Blank[7] LCS[1] LCSD[1] 332404852-0021 03/22/2410:09 03/22/2411:20 03/22/2410:12 03/22/2410:14 03/22/2413:30 Result Ng/filter RL Ng/filter Result pg/filter RL Ng/filter Result pg/filter True Conc jig/filter % Rec 73.7051-119. 552 Result pg/filter True Conc jig/filter % Rec 73.7051-119. 552 % RPD <m20 RL pg/m' Result Ng/m' Aluminum -1.00 5. -0.280 5.0 22.9 25.0 91.6 22.9 25.0 91.8 0.196 3. -0.13 Antimony -0.205 1.0 0.280 1.0 23.1 25.0 92.4 23.1 25.0 92.3 0.130 0.71 -0.067 Arsenic 0.20 1. -0.280, 1.0 22.2 25.0 88.8 22.8 25.0 91.2 2.71 0.71 -0.021 Barium 0.0050 5. 0.010 5.0 23.4 25. 93.4 23.3 25.0 93.1 0.322 3.5 0.035 Beryllium 0.00500 0.11C 0.0050 0.1 23.7 25. 94.6 23.5 25.0 94.0 0.721 0.071 0.0 Cadmium 0.0150 0.2C 0.0 0.2 24.5 25. 97.8 25.0 25.0 100 2.28 0.14 0.010 Chromium -0.020 1. -0.015 1. 23.6 25. 94.3 23.5 25.0 94.1 0.212 0.71 0.0141 Cobalt 0.0100 0.50 0.015 0.5 25.1 25.0 100 25.7 25.0 103 2.15 0.35 0.017 Copper 0.0250 1.0 0.035 1. 24.6 25.0 98.5 24.4 25.0 97.4 1.08 0.71 0.18 Lead -0.085 0.5 -0.25 0.5 23.5 25.0 93.8 23.8 25.0 95.1 1.33 0.3 -0.045 Manganese -0.00500 0.50 0.0050 0.5 24.8 25.0 99.2 24.6 25.0 98.5 0.72q 0.35 0.010 Molybdenum 0.0300 0.50 0.010 0.5 24.9 25.0 99.5 25.5 25.0 102 2.38 0.3 -0.0035 Nickel 0.0200 1.0 0.030 1. 25.3 25.0 101 25.8 25.0 103 1.98 0.71 0.035 Selenium 0.160 1.0 0.42 1. 23.0 25.0 92.2 23.8 25.0 95.2 3.25 0.71 0.25 Silver 0.0150 1.0 0.015 1. 23.3 25.0 93.2 23.2 25.0 92.7 0.560 0.71 0.021 Thallium 0.0750 1.0 0.080 1. 24.1 25.0 96.5 24.5 25.0 98.1 1.64 0.71 0.070 Vanadium -0.0300 0.50 0.010 0.5 24.1 25.0 96.5 23.9 25.0 95.81 0.74 0.3 -0.031 Zinc -0.060 1. -0.045 1. 24.q 25.q 99.3 25.4 25.0 102 2.411 0.71 0.0811 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 1 of 2 Page 22 Of 30 Printed Batch: Instrument: Initial Cal Std: Cal Check Std: Internal Std: LCS Std MS Std Matrix: 3/25/2024 33Q240321-6MCE 33-PE8300 Cassettes Other 332404852-0022 03/22/24 13:32 RL pg/filter Result pg/filter Aluminum 5. 0.090 Antimony 1. -0.15 Arsenic 1. -0.27 Barium 5.0 0.025 Beryllium 0.10 0.0 Cadmium 0.20 0.020 Chromium 1.0 0.025 Cobalt 0.50 0.0050 Copper 1.0 0.18 Lead 0.5 -0.14 Manganese 0.50 0.010 Molybdenum 0.50 0.025 Nickel 1.0 0.015 Selenium 1.0 0.085 Silver 1.0 0.040 Thallium 1.0 0.25 Vanadium 0.50 0.010 Zinc 1.0 0.10 ICP QC Batch Summary Created: 3/21/24 2:09 pm By: xle 332404846-0021 332404982-0021 332404846-0022 332404982-0022 332404852-0021 332404987-0021 332404852-0022 332404987-0022 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 2 of 2 Page 23 Of 30 OrderID: 332404852 w r cr z c c c c c c c c c c �r m n n n n n n n n n n n n n n n n n > n nlu Qn Z 0 0W 0 0 0 o 0 o 0 0 3 r -a 3 0 _K CL3 m m O m O m O m m 0 m O m 0 m c m 0 m O r n� rr O O Q 0 0 0 Q 0 0 - O co 0 LD 00 V Ol Ln � w fv 1--+ O D D D D D D D D D D nn i .r O 4 CL Ln _ i m 0 m 0 m 0 rn o m 0 m Q m 0 m 0 rn 0 m 0 r* 41 0 3 O m � O 0 LD 0 00 0 �l 0 M 0 Ln 0 A 0 W 0 N o 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N Q m ❑ rD ro - � 3 ❑■ 0 q m S T O M m 0 0 w N N N tD co D z n a m n n n n z 0 T n /c V 0 v D z v n z n cn A m 0 X r*0 w w N 0 00 VI 1V LA Testing 5431 Industrial Drive, Huntington Beach, CA 92649 /Pir Phone: (714) 828-4999 Fax: (714) 828-4944 I Email: hblab@latesting.com TESTING Attn: Noah Ambos Customer ID: CTEH99 CTEH Center for Toxicology & Env. Health Customer PO: 5120 North Shore Drive Received: 03/18/24 10:45 AM North Little Rock, AR 72118 Fax: (501) 614-2835 Phone: (501) 454-1622 LA Testing Order: 332404852 Project: PRO7-032229 LA Testing Proj ID: PROJ-032229 Cust COC ID Project Type: Standard Project Receipt Confirmation Shipping Tracking Number: EMSL Received Cust Sample Order ID Test Date TAT Due Date TUCA0317ME001A 332404852-0001 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME001A 332404852-0001 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME002A 332404852-0002 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME002A 332404852-0002 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME003A 332404852-0003 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME003A 332404852-0003 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME004A 332404852-0004 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME004A 332404852-0004 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME005A 332404852-0005 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME005A 332404852-0005 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME006A 332404852-0006 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME006A 332404852-0006 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME007A 332404852-0007 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM Date Sent 311812024 4:16:02 PM Paqe 27 Of 30 1 911ALA Testing 5431 Industrial Drive, Huntington Beach, CA 92649 Phone: (714) 828-4999 Fax: (714) 828-4944 Email: hblab@latesting.com TESTING Attn: Noah Ambos Customer ID: CTEH99 CTEH Center for Toxicology & Env. Health Customer PO: 5120 North Shore Drive North Little Rock, AR 72118 Received: 03/18/24 10:45 AM Fax: (501) 614-2835 Phone: (501) 454-1622 LA Testing Order: 332404852 Project: PRO7-032229 LA Testing Proj ID: PROJ-032229 Cust COC ID Project Type: Standard Project Receipt Confirmation Shipping Tracking Number: EMSL Received Cust Sample Order ID Test Date TAT Due Date TUCA0317ME007A 332404852-0007 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME008A 332404852-0008 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME008A 332404852-0008 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME009A 332404852-0009 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME009A 332404852-0009 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME010A 332404852-0010 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME010A 332404852-0010 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317MEFBO01A 332404852-0011 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317MEFBO01A 332404852-0011 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME001B 332404852-0012 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME001B 332404852-0012 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME002B 332404852-0013 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME002B 332404852-0013 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM Date Sent 311812024 4:16:02 PM Paqe 28 Of 30 2 911ALA Testing 5431 Industrial Drive, Huntington Beach, CA 92649 Phone: (714) 828-4999 Fax: (714) 828-4944 Email: hblab@latesting.com TESTING Attn: Noah Ambos Customer ID: CTEH99 CTEH Center for Toxicology & Env. Health Customer PO: 5120 North Shore Drive North Little Rock, AR 72118 Received: 03/18/24 10:45 AM Fax: (501) 614-2835 Phone: (501) 454-1622 LA Testing Order: 332404852 Project: PRO7-032229 LA Testing Proj ID: PROJ-032229 Cust COC ID Project Type: Standard Project Receipt Confirmation Shipping Tracking Number: EMSL Received Cust Sample Order ID Test Date TAT Due Date TUCA0317ME003B 332404852-0014 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME003B 332404852-0014 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME004B 332404852-0015 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME004B 332404852-0015 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME005B 332404852-0016 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME005B 332404852-0016 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME006B 332404852-0017 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME006B 332404852-0017 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME007B 332404852-0018 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME007B 332404852-0018 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME008B 332404852-0019 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME008B 332404852-0019 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME009B 332404852-0020 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM Date Sent 311812024 4:16:02 PM Paqe 29 Of 30 3 911ALA Testing 5431 Industrial Drive, Huntington Beach, CA 92649 Phone: (714) 828-4999 Fax: (714) 828-4944 Email: hblab@latesting.com TESTING Attn: Noah Ambos Customer ID: CTEH99 CTEH Center for Toxicology & Env. Health Customer PO: 5120 North Shore Drive North Little Rock, AR 72118 Received: 03/18/24 10:45 AM Fax: (501) 614-2835 Phone: (501) 454-1622 LA Testing Order: 332404852 Project: PRO7-032229 LA Testing Proj ID: PROJ-032229 Cust COC ID Project Type: Standard Project Receipt Confirmation Shipping Tracking Number: EMSL Received Cust Sample Order ID Test Date TAT Due Date TUCA0317ME009B 332404852-0020 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME010B 332404852-0021 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317ME010B 332404852-0021 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317MEFBO01B 332404852-0022 C-CAM 16 Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM TUCA0317MEFBO01B 332404852-0022 C-Metals by ICP 3/18/2024 1 Week (EOD) 3/25/2024 10:45:00 AM 6:00:00 PM Note: The above sample log -in information is based solely on the data provided by the customer on the Chain of Custody form. Sample count, ID number verification, and evaluation of each individual sample is not started/done until sample analysis process begins by the scientist at the lab bench. If at this point the staff finds that a sample is missing, ID number does not match, or has any other issue that will disrupt analysis, the customer will be notified. Date Sent 311812024 4:16:02 PM Paqe 30 Of 30 4