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HomeMy WebLinkAboutMetals 03212024LA TESTING 1"j'A TESTING Noah Ambos CTEH Center for Toxicology & Env. Health 5120 North Shore Drive North Little Rock, AR 72118 LA Testing 5431 Industrial Drive Huntington Beach, CA 92649 (714) 828-4999 CustomerService(o)emsl.com Re: Narrative: NIOSH 7303 LA Testing Order: 332405230, Project ID: PROJ-032229 Dear Noah HUNTINGTON BEACH, CA 92649 5431 INDUSTRIAL DRIVE PHONE: (714) 828-4999 On 3/22/2024, LA Testing Huntington Beach, CA received 22 air samples for metals analysis via NIOSH 7300 Modified method. The samples were received and logged in following normal lab procedures. All samples were received under Chain of Custody and in good condition unless otherwise noted. NIOSH 7300 Modified LA Testing Order: 332405230, Project ID: PROJ-032229: All samples were prepared and analyzed according to the method specified NIOSH 7300 Modified. The samples were submitted on cellulose ester membrane filters which were prepared utilizing a hot block digestion technique as indicated in the method. The samples were then analyzed via Inductively Coupled Plasma (ICP) analysis utilizing Atomic Emission Spectroscopy (AES). All preparation and analyses were performed within the method specific hold time requirement. Results are reported in mg/m3. Quality Control Dilutions: None Calibrations: The RL, RLVS ICV and bracketing CCV standards were within control limits. Blanks: Target analytes were not detected above the reporting limit in the associated blanks. Media blank was not subtracted from sample concentrations. LCS/LCSD: The laboratory control sample spike recoveries and RPD results were within control limits. ICSA/ICSB: The interference check solution results were within control limits. QC was performed at rates compliant with both the American Industrial Hygiene Association (AIHA) and the California Environmental Laboratory Accreditation Program (ELAP). 1 certify that this report is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. In addition, I certify, that to the best of my knowledge and belief, the data as reported are true and accurate. Release of the data contained in this Michael Chapman, Laboratory Manager q• Paqe 1 Of April 01, 2024 CHEMMETALNARR.2.0 LA Testing 5431 Industrial Drive, Huntington Beach, CA 92649 Phone: (714) 828-4999 Fax: (714) 828-4944 Email: hblabOlatestinq.com TESTING Attn: Noah Ambos 4/1/2024 CTEH Center for Toxicology & Env. Health 5120 North Shore Drive North Little Rock, AR 72118 Phone: (501) 801-8500 Fax: (501) 614-2835 The following analytical report covers the analysis performed on samples submitted to LA Testing on 3/22/2024. The results are tabulated on the attached data pages for the following client designated project: Project ID: PROJ-032229 PROJ-032229 The reference number for these samples is EMSL Order #332405230. Please use this reference when calling about these samples. If you have any questions, please do not hesitate to contact me at (714) 828-4999. Approved By: Michael Chapman, Laboratory Manager AIHA LAP, LLC-IHLAP Accredited #101650 EMSL maintains liability limited to cost of analysis. Interpretation and use of test results are the responsibility of the client. This report relates only to the samples reported above, and may not be reproduced, except in full, without written approval by EMSL. EMSL bears no responsibility for sample collection activities or analytical method limitations. The report reflects the samples as received. Results are generated from the field sampling data (sampling volumes and areas, locations, etc.) provided by the client on the Chain of Custody. Samples are within quality control criteria and met method specifications unless otherwise noted. Page 1 of 16 Paqe 2 Of 30 LA Testing LA Testing Order: 332405230 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/22/2024 10:35 AM North Little Rock, AR 72118 Collected: 3/21/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0321 ME001A Collected. 3/21/2024 Lab ID: 332405230-0001 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.070 0.070 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH Client Sample Description TUCA0321 ME002A Collected. 3/21/2024 Lab ID: 332405230-0002 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.070 0.070 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 4/1/2024 1:39:10 PM Page 2 of 16 Paqe 3 Of 30 LA Testing LA Testing Order: 332405230 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/22/2024 10:35 AM North Little Rock, AR 72118 Collected: 3/21/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0321 ME002A Collected. 3/21/2024 Lab ID: 332405230-0002 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH Client Sample Description TUCA0321 ME003A Collected. 3/21/2024 Lab ID: 332405230-0003 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.8 3.8 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.76 0.76 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.76 0.76 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.8 3.8 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.076 0.076 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.15 0.15 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.76 0.76 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.38 0.38 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.76 0.76 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.38 0.38 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.38 0.38 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Molybdenum <0.38 0.38 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.76 0.76 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.76 0.76 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.76 0.76 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.76 0.76 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.38 0.38 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.76 0.76 pg/m' 3/28/2024 CM 3/29/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 4/1/2024 1:39:10 PM Page 3 of 16 Paqe 4 Of 30 LA Testing LA Testing Order: 332405230 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/22/2024 10:35 AM North Little Rock, AR 72118 Collected: 3/21/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0321 ME004A Collected. 3/21/2024 Lab ID: 332405230-0004 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.070 0.070 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH Client Sample Description TUCA0321 ME005A Collected. 3/21/2024 Lab ID: 332405230-0005 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.070 0.070 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 4/1/2024 1:39:10 PM Page 4 of 16 Paqe 5 Of 30 LA Testing LA Testing Order: 332405230 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/22/2024 10:35 AM North Little Rock, AR 72118 Collected: 3/21/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0321 ME005A Collected. 3/21/2024 Lab ID: 332405230-0005 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH Client Sample Description TUCA0321 ME006A Collected. 3/21/2024 Lab ID: 332405230-0006 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.070 0.070 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 4/1/2024 1:39:10 PM Page 5 of 16 Paqe 6 Of 30 LA Testing LA Testing Order: 332405230 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/22/2024 10:35 AM North Little Rock, AR 72118 Collected: 3/21/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0321 ME007A Collected. 3/21/2024 Lab ID: 332405230-0007 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.070 0.070 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH Client Sample Description TUCA0321 ME008A Collected. 3/21/2024 Lab ID: 332405230-0008 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.070 0.070 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 4/1/2024 1:39:10 PM Page 6 of 16 Paqe 7 Of 30 LA Testing LA Testing Order: 332405230 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/22/2024 10:35 AM North Little Rock, AR 72118 Collected: 3/21/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0321 ME008A Collected. 3/21/2024 Lab ID: 332405230-0008 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH Client Sample Description TUCA0321 ME009A Collected. 3/21/2024 Lab ID: 332405230-0009 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <4.2 4.2 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.85 0.85 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.85 0.85 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <4.2 4.2 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.085 0.085 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.17 0.17 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.85 0.85 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.42 0.42 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.85 0.85 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.42 0.42 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.42 0.42 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Molybdenum <0.42 0.42 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.85 0.85 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.85 0.85 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.85 0.85 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.85 0.85 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.42 0.42 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.85 0.85 pg/m' 3/28/2024 CM 3/29/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 4/1/2024 1:39:10 PM Page 7 of 16 Paqe 8 Of 30 LA Testing LA Testing Order: 332405230 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/22/2024 10:35 AM North Little Rock, AR 72118 Collected: 3/21/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0321 ME010A Collected. 3/21/2024 Lab ID: 332405230-0010 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.070 0.070 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH Client Sample Description TUCA0321 MEFBO01A Collected. 3/21/2024 Lab ID: 332405230-0011 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <5.0 5.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <5.0 5.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.10 0.10 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.20 0.20 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.50 0.50 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.50 0.50 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.50 0.50 pg/filter 3/28/2024 CM 3/29/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 4/1/2024 1:39:10 PM Page 8 of 16 Paqe 9 Of 30 LA Testing LA Testing Order: 332405230 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/22/2024 10:35 AM North Little Rock, AR 72118 Collected: 3/21/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0321 MEFBO01A Collected. 3/21/2024 Lab ID: 332405230-0011 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.50 0.50 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.50 0.50 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH Client Sample Description TUCA0321 ME001 B Collected. 3/21/2024 Lab ID: 332405230-0012 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.4 3.4 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.4 3.4 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.069 0.069 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Molybdenum <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 4/1/2024 1:39:10 PM Page 9 of 16 Paqe 10 Of 30 LA Testing LA Testing Order: 332405230 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/22/2024 10:35 AM North Little Rock, AR 72118 Collected: 3/21/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0321 ME002B Collected. 3/21/2024 Lab ID: 332405230-0013 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.4 3.4 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.4 3.4 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.069 0.069 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Molybdenum <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH Client Sample Description TUCA0321 ME003B Collected. 3/21/2024 Lab ID: 332405230-0014 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.4 3.4 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.4 3.4 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.069 0.069 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 4/1/2024 1:39:10 PM Page 10 of 16 Paqe 11 Of 30 LA Testing LA Testing Order: 332405230 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/22/2024 10:35 AM North Little Rock, AR 72118 Collected: 3/21/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0321 ME003B Collected. 3/21/2024 Lab ID: 332405230-0014 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH Client Sample Description TUCA0321 ME004B Collected. 3/21/2024 Lab ID: 332405230-0015 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.4 3.4 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.4 3.4 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.069 0.069 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Molybdenum <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.34 0.34 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 4/1/2024 1:39:10 PM Page 11 of 16 Paqe 12 Of 30 LA Testing LA Testing Order: 332405230 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/22/2024 10:35 AM North Little Rock, AR 72118 Collected: 3/21/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0321 ME005B Collected. 3/21/2024 Lab ID: 332405230-0016 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.069 0.069 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH Client Sample Description TUCA0321 ME006B Collected. 3/21/2024 Lab ID: 332405230-0017 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.069 0.069 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 4/1/2024 1:39:10 PM Page 12 of 16 Paqe 13 Of 30 LA Testing LA Testing Order: 332405230 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/22/2024 10:35 AM North Little Rock, AR 72118 Collected: 3/21/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0321 ME006B Collected. 3/21/2024 Lab ID: 332405230-0017 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH Client Sample Description TUCA0321 ME007B Collected. 3/21/2024 Lab ID: 332405230-0018 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.069 0.069 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.69 0.69 pg/m' 3/28/2024 CM 3/29/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 4/1/2024 1:39:10 PM Page 13 of 16 Paqe 14 Of 30 LA Testing LA Testing Order: 332405230 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/22/2024 10:35 AM North Little Rock, AR 72118 Collected: 3/21/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0321 ME008B Collected. 3/21/2024 Lab ID: 332405230-0019 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <5.1 5.1 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <1.0 1.0 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <1.0 1.0 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <5.1 5.1 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.10 0.10 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.20 0.20 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <1.0 1.0 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.51 0.51 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <1.0 1.0 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.51 0.51 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.51 0.51 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Molybdenum <0.51 0.51 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <1.0 1.0 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <1.0 1.0 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <1.0 1.0 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <1.0 1.0 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.51 0.51 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <1.0 1.0 pg/m' 3/28/2024 CM 3/29/2024 TH Client Sample Description TUCA0321 ME009B Collected. 3/21/2024 Lab ID: 332405230-0020 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.070 0.070 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 4/1/2024 1:39:10 PM Page 14 of 16 Paqe 15 Of 30 LA Testing LA Testing Order: 332405230 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/22/2024 10:35 AM North Little Rock, AR 72118 Collected: 3/21/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0321 ME009B Collected. 3/21/2024 Lab ID: 332405230-0020 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH Client Sample Description TUCA0321 ME010B Collected. 3/21/2024 Lab ID: 332405230-0021 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <3.5 3.5 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.070 0.070 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.14 0.14 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Molybdenum <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.35 0.35 pg/m' 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <0.70 0.70 pg/m' 3/28/2024 CM 3/29/2024 TH ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 4/1/2024 1:39:10 PM Page 15 of 16 Paqe 16 Of 30 LA Testing LA Testing Order: 332405230 CustomerlD: CTEH99 5431 Industrial Drive, Huntington Beach, CA 92649 CustomerPO: APhone/Fax: (714) 828-4999 / (714) 828-4944 TESTING http://www.LATestina.com hblab(a latestina.com ProjectlD: PROJ-032229 Attn: Noah Ambos Phone: (501) 801-8500 CTEH Center for Toxicology & Env. Health Fax: (501) 614-2835 5120 North Shore Drive Received: 3/22/2024 10:35 AM North Little Rock, AR 72118 Collected: 3/21/2024 PROJ-032229 Analytical Results Client Sample Description TUCA0321 MEFBO01 B Collected. 3/21/2024 Lab ID: 332405230-0022 Prep Analysis Method Parameter Result RL Units Date & Analyst Date & Analyst METALS 7300 Modified Aluminum <5.0 5.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Antimony <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Arsenic <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Barium <5.0 5.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Beryllium <0.10 0.10 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Cadmium <0.20 0.20 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Chromium <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Cobalt <0.50 0.50 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Copper <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Lead <0.50 0.50 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Manganese <0.50 0.50 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Molybdenum <0.50 0.50 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Nickel <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Selenium <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Silver <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Thallium <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Vanadium <0.50 0.50 pg/filter 3/28/2024 CM 3/29/2024 TH 7300 Modified Zinc <1.0 1.0 pg/filter 3/28/2024 CM 3/29/2024 TH AIHA LAP, LLC-IHLAP Accredited #101650 Definitions: MDL - method detection limit J - Result was below the reporting limit, but at or above the MDL ND - indicates that the analyte was not detected at the reporting limit RL - Reporting Limit (Analytical) D - Dilution Sample required a dilution which was used to calculate final results ChemSmplw/RDL/NELAC-2.19.0.0 Printed: 4/1/2024 1:39:10 PM Page 16 of 16 Paqe 17 Of 30 Printed: 4/1 /2024 Batch: 33Q240328-1 MICE Instrument: 33-PE8300 Initial Cal Std: Cal Check Std: Internal Std: LCS Std MS Std Matrix: Cassettes I ICP QC Batch Summary Created: 3/28/24 11:22 am By: camartinez 332405230-0001 332405230-0005 332405230-0009 332405230-0013 332405230-0017 332405230-0002 332405230-0006 332405230-0010 332405230-0014 332405230-0018 332405230-0003 332405230-0007 332405230-0011 332405230-0015 332405230-0019 332405230-0004 332405230-0008 332405230-0012 332405230-0016 332405230-0020 Blank/DL Control Other Method Blank[7] Matrix Blank[7] LCS[1] LCSD[1] 332405230-0001 03/29/24 09:46 03/29/24 09:49 03/29/24 09:51 03/29/24 09:54 03/29/24 10:10 Result Ng/filter RL Ng/filter Result pg/filter RL Ng/filter Result pg/filter True Conc jig/filter % Rec 73.7051-119. 552 Result pg/filter True Conc pg/filter % Rec 73.7051-119. 552 % RPD <m20 RL pg/m' Result Ng/m' Aluminum 0.130 5. -0.320 5.0 22.7 25.0 90.7 22.6 25.0 90.2 0.508 3.5 0.23 Antimony -0.89 1. -1.07 1.0 22.9 25.0 91.6 23.1 25.0 92.6 1.11 0.7 -0.045 Arsenic -0.27 1. -0.0800, 1.0 23.0 25.0 92.0 23.3 25.0 93.0 1.10 0.70 0.0035 Barium 0.0 5. -0.0050 5.0 23.5 25. 94.0 23.8 25.0 95.1 1.21 3.5 0.017 Beryllium 0.00 0.11C 0.0050 0.1 23.0 25. 92.1 23.5 25.0 94.0 2.02 0.070 0.0 Cadmium -0.00500 0.2C 0.0050 0.2 24.3 25. 97.3 25.9 25.0 104 6.25 0.14 0.0070 Chromium -0.015 1. 0.0050 1. 24.9 25. 99.7 25.2 25.0 101 0.918 0.70 0.049 Cobalt -0.050 0.5 -0.025 0.5 26.5 25. 106 26.7 25.0 107 0.808 0.3 -0.021 Copper 0.00 1. -0.030 1. 26.1 25. 105 26.5 25.0 106 1.52 0.70 0.26 Lead 0.0650 0.5 -0.010 0.50 24.4 25. 97.7 24.5 25.0 97.9 0.241 0.35 0.010 Manganese -0.010 0.5 -0.0050 0.50 24.9 25. 99.0 25.2 25.0 101 1.06 0.35 0.028 Molybdenum 0.0600 0.50 0.020 0.50 25.8 25.0 103 25.9 25.0 104 0.600 0.35 0.017 Nickel 0.00 1.0 0.0050 1.0 25.3 25. 101 25.5 25.0 102 0.748 0.70 0.017 Selenium -0.045 1. -0.35 1.0 23.3 25. 93.3 23.5 25.0 94.0 0.769 0.7 -0.33 Silver 0.0100 1.0 0.040q 1.q 25.0 25. 100 25.5 25.0 102 1.68 0.70 0.031 Thallium 0.045 1. -0.11 1. 25.0 25. 100 25.2 25.0 101 0.7771 0.7 -0.12 Vanadium -0.0250 0.50 0.010 0.5 25.3 25.9 101 25.7 25.0 103 1.3 0.3 -0.014 Zinc 0.015q 1.0 0.010 1. 26.q 25.0 106 26.6 25.0 107 0.6411 0.7q 0.25 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 1 of 4 Page 18 Of 30 Printed: 4/1/2024 ICP QC Batch Summary Batch: 33Q240328-1 MICE Created: 3/28/24 11:22 am By: camartinez Instrument: 33-PE8300 Initial Cal Std: Samples: Cal Check Std: Internal Std: 332405230-0001 332405230-0005 332405230-0009 LCS Std 332405230-0002 332405230-0006 332405230-0010 332405230-0003 332405230-0007 332405230-0011 MS Std 332405230-0004 332405230-0008 332405230-0012 Matrix: Cassettes 332405230-0013 332405230-0017 332405230-0014 332405230-0018 332405230-0015 332405230-0019 332405230-0016 332405230-0020 Other 332405230-0002 332405230-0003 332405230-0004 332405230-0005 332405230-0006 332405230-0007 332405230-0008 03/29/2410:13 03/29/2410:16 03/29/2410:18 03/29/2410:21 03/29/2410:23 03/29/2410:31 03/29/2410:33 RL pg/m' Result Ng/m3 RL pg/m' Result Ng/m' RL pg/m' Result Ng/m' RL pg/m' Result pg/m' RL pg/m' Result Ng/m' RL pg/m' Result pg/m' RL pg/m' Result Ng/m' Aluminum 3.5 0.252 3.8 0.328 3. 0.23 3.5 0.517 3.5 0.470 3. -0.130 3.5 0.55 Antimony 0.7 -0.151 0.7 -0.301 0.7 -0.56z 0.70 -0.816 0.70 -0.417 0.70 -0.694 0.70 0.0421 Arsenic 0.7 -0.158 0.7 -0.221 0.7 -0.013 0.70 -0.183 0.70 -0.207 0.7 -0.0736 0.70 0.038 Barium 3.5 0.0245 3.8 0.0191 3.5 0.0209 3.5 0.0211 3.5 0.0210 3.5 0.0210 3.5 0.021 Beryllium 0.070 0.00 0.076 0.00 0.070 0.00 0.070 0.00 0.070 0.00 0.070 0.00 0.070 0.0 Cadmium 0.14 0.00350 0.15 0.00381 0.14 0.0104 0.14 0.00 0.14 0.0140 0.14 0.0105 0.14 0.00351 Chromium 0.70 0.0491 0.76 0.0610 0.70 0.0313 0.70 0.225 0.70 0.158 0.70 0.0315 0.70 0.024 Cobalt 0.3 -0.00350 0.38 0.0076 0.3 -0.017 0.3 -0.0176 0.3 -0.010 0.3 -0.017 0.3 -0.014 Copper 0.70 0.245 0.7q 0.229 0.70 0.240 0.7q 0.215 0.70 0.242 0.7q 0.270 0.70 0.29 Lead 0.35 0.0245 0.3 -0.0114 0.35 0.00348 0.35 0.00352 0.3 -0.0245 0.35 0.0385 0.3 -0.091 Manganese 0.35 0.0315 0.38 0.0229 0.35 0.0209 0.35 0.0246 0.35 0.0351 0.35 0.0245 0.35 0.021 Molybdenum 0.35 0.0350 0.38 0.00381 0.35 0.0174 0.35 0.00 0.3 -0.0105 0.35 0.00701 0.35 0.0351 Nickel 0.70 0.0140 0.76 0.0229 0.7 0.00697 0.70 0.0387 0.70 0.0281 0.70 0.0245 0.70 0.017 Selenium 0.7 -0.224 0.7 -0.343 0.7 0.0418 0.70 -0.010 0.70 -0.017 0.7 -0.228 0.7 -0.55 Silver 0.70 0.00350 0.7q 0.02671 0.7 0.0348 0.70 0.0176 0.70 0.00 0.701 0.00701 0.70 0.024 Thallium 0.7 -0.045 0.7 -0.17 0.7 -0.090 0.70 -0.0492 0.70 -0.0245 0.70 0.0455 0.7 -0.0561 Vanadium 0.35 0.00 0.38 0.00763 0.3 0.00 0.35 0.00352 0.3 -0.017 0.3 -0.010 0.3 -0.00351 Zinc 0.7q 0.259 0.76 0.214 0.7q 0.237 0.70 0.190 0.70 0.221 0.70 0.259 0.70 0.231 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 2 of 4 Page 19 Of 30 Printed: 4/1/2024 ICP QC Batch Summary Batch: 33Q240328-1 MICE Created: 3/28/24 11:22 am By: camartinez Instrument: 33-PE8300 Initial Cal Std: Samples: Cal Check Std: Internal Std: 332405230-0001 332405230-0005 332405230-0009 LCS Std 332405230-0002 332405230-0006 332405230-0010 332405230-0003 332405230-0007 332405230-0011 MS Std 332405230-0004 332405230-0008 332405230-0012 Matrix: Cassettes 332405230-0013 332405230-0017 332405230-0014 332405230-0018 332405230-0015 332405230-0019 332405230-0016 332405230-0020 Other 332405230-0009 332405230-0010 332405230-0011 332405230-0012 332405230-0013 332405230-0014 332405230-0015 03/29/2410:36 03/29/2410:39 03/29/2410:41 03/29/2410:44 03/29/2410:46 03/29/2410:49 03/29/2410:52 RL Ng/m' me Result Ng/m' RL Ng/m' Result Ng/m' RL Ng/filter Result N9/filter RL Ng/m' Result N9/m' RL Ng/m' Result N9/m' RL Ng/m' Result N9/m' RL Ng/m' Result N9/m' Aluminum 4.2 0.394 3.5 0.332 5. -0.120 3.4 0.441 3.4 0.148 3.4 0.217 3. -0.0034 Antimony 0.8 -0.233 0.7 -0.59 1. -0.520 0.69 -0.386 0.69 -0.213 0.6 -0.420 0.6 -0.69 Arsenic 0.8 -0.0382 0.70, 0.164 1. -0.040 0.69 -0.241 0.69 0.0620 0.6 -0.210 0.6 -0.16 Barium 4.2 0.0212 3.5 0.0245 5.0 0.015 3. 0.0241 3.4 0.0241 3.4 0.0241 3.4 0.017 Beryllium 0.085 0.00 0.070 0.00 0.1 0.0 0.06 0.00 0.069 0.00 0.069 0.00 0.069 0.0 Cadmium 0.17 0.00848 0.14 0.00699 0.2C 0.010 0.14 0.00 0.14 0.00344 0.14 0.00 0.14 0.0 Chromium 0.85 0.293 0.70 0.0384 1.0 0.040 0.69 0.0344 0.69 0.220 0.69 0.0275 0.69 0.031 Cobalt 0.4 -0.012 0.3 -0.0069 0.5 -0.020C 0.34 0.00344 0.34 -0.020 0.3 -0.0172 0.34 0.0068 Copper 0.85 0.288 0.7q 0.206 1.0 0.27C 0.69 0.227 0.69 0.182 0.69 0.230 0.69 0.20 Lead 0.42 0.0339 0.3 -0.0105 0.5c 0.015C 0.34 -0.0827 0.34 -0.0929 0.3 0.0688 0.3 -0.0551 Manganese 0.42 0.0254 0.35 0.0245 0.5C 0.015C 0.34 0.0241 0.34 0.0207 0.34 0.0206 0.34 0.017 Molybdenum 0.42 0.0467 0.35 0.0245 0.5C 0.010C 0.34 0.0310 0.34 0.00344 0.3 -0.0103 0.34 0.0068 Nickel 0.85 0.0339 0.70 0.0175 1.0 0.030C 0.69 0.0172 0.69 0.0275 0.69 0.0138 0.69 0.020 Selenium 0.85 0.0551 0.7 -0.36 1. -0.26C 0.69 -0.472 0.6 -0.258 0.6 -0.420 0.6 -0.28 Silver 0.85 0.0251 0.7q 0.014q 1.0 0.025C 0.69 0.0482 0.69 0.0310 0.69 0.0309 0.69 0.0241 Thallium 0.8 -0.12 0.7 -0.196 1.0 0.030C 0.69 -0.0689 0.69 0.0482 0.6 -0.0722 0.6 -0.041 Vanadium 0.4 -0.00848 0.3 0.0069 0.5 -0.0050 0.34 -0.00689 0.34 0.013 0.34 -0.0172 0.3 0.013 Zinc 0.8 0.25 0.7 0.20 1. 0.23 0.69 0.193 0.69 0.182 0.60 0.1821 0.69 0.23 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 3 of 4 Page 20 Of 30 Printed: 4/1/2024 ICP QC Batch Summary Batch: 33Q240328-1 MICE Created: 3/28/24 11:22 am By: camartinez Instrument: 33-PE8300 Initial Cal Std: Samples: Cal Check Std: Internal Std: 332405230-0001 332405230-0005 332405230-0009 LCS Std 332405230-0002 332405230-0006 332405230-0010 332405230-0003 332405230-0007 332405230-0011 MS Std 332405230-0004 332405230-0008 332405230-0012 Matrix: Cassettes 332405230-0013 332405230-0017 332405230-0014 332405230-0018 332405230-0015 332405230-0019 332405230-0016 332405230-0020 Other 332405230-0016 332405230-0017 332405230-0018 332405230-0019 332405230-0020 03/29/2410:54 03/29/2411:02 03/29/2411:04 03/29/2411:07 03/29/2411:09 RL pg/m' Result Ng/m3 RL pg/m' Result Ng/m' RL pg/m' Result Ng/m' RL pg/m' Result pg/m' RL pg/m' Result Ng/m' Aluminum 3.5 0.518 3.5 0.107 3. 0.47E 5.1 0.327 3.5 0.157 Antimony 0.6 -0.935 0.6 -0.49 0.6 -0.54 1.0 -0.643 0.70 -0.947 Arsenic 0.69 0.142 0.6 -0.024 0.6 -0.066 1.0 -0.199 0.70 -0.153 Barium 3.5 0.0242 3.5 0.0242 3.5 0.0174 5.1 0.0357 3.5 0.0244 Beryllium 0.069 0.00 0.069 0.00 0.069 0.00 0.10 0.00 0.070 0.00 Cadmium 0.14 0.00 0.14 0.00346 0.14 0.00694 0.20 0.00510 0.14 -0.00696 Chromium 0.69 0.231 0.69 0.0346 0.69 0.0278 1.0 0.0561 0.70 0.0313 Cobalt 0.3 -0.0069 0.3 -0.010 0.3 -0.013 0.51 -0.045 0.3 -0.013 Copper 0.69 0.224 0.6q 0.208 0.69 0.219 1.0 0.270 0.70 0.212 Lead 0.35 0.0759 0.35 0.0415 0.3 -0.0069 0.51 -0.0255 0.35 0.00348 Manganese 0.35 0.0207 0.35 0.0208 0.35 0.0174 0.51 0.0204 0.35 0.0174 Molybdenum 0.35 0.0207 0.35 0.0242 0.3 -0.0104 0.51 0.0306 0.35 0.013 Nickel 0.69 0.0207 0.69 0.0138 0.69 0.0104 1.0 0.0255 0.70 0.0174 Selenium 0.6 -0.0311 0.6 -0.15 0.6 -0.038 1.0 -0.694 0.70 -0.272 Silver 0.69 0.0173 0.6q 0.0173 0.6 0.0278 1.0 0.0255 0.70 0.00348 Thallium 0.6 -0.048 0.6 -0.069 0.6 -0.12 1.0 -0.138 0.70 -0.020 Vanadium 0.35 0.00 0.35 0.020 0.3 0.00 0.51 0.0255 0.35 0.00 Zinc 0.69 0.204 0.69 0.19g 0.6 0.236 1.0 0.245 0.70 0.18 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 4 of 4 Page 21 Of 30 Printed: 4/1 /2024 Batch: 33Q240328-2MC E Instrument: 33-PE8300 Initial Cal Std: Cal Check Std: Internal Std: LCS Std MS Std Matrix: Cassettes I ICP QC Batch Summary Created: 3/28/24 11:26 am By: camartinez 332404864-0001 332404864-0005 332405230-0022 332405564-0004 332405564-0008 332404864-0002 332404864-0006 332405564-0001 332405564-0005 332405564-0009 332404864-0003 332404864-0007 332405564-0002 332405564-0006 332405564-0010 332404864-0004 332405230-0021 332405564-0003 332405564-0007 Blank/DL Control Other Method Blank[7] Matrix Blank[7] LCS[1] LCSD[1] 332405230-0021 03/29/24 10:01 03/29/24 10:03 03/29/24 10:06 03/29/24 10:08 03/29/24 11:12 Result Ng/filter RL Ng/filter IL Result pg/filter RL Ng/filter Result pg/filter True Conc jig/filter % Rec 73.7051-119. 552 Result pg/filter True Conc jig/filter % Rec 73.7051-119. 552 % RPD <m20 RL pg/m3 Result Ng/m' Aluminum -0.42 5. -0.0600 5.0 24.2 25.0 96.9 24.1 25.0 96.6 0.269 3.5 0.37 Antimony -0.50 1. -0.705 1.0 24.4 25.0 97.6 24.7 25.0 99.0 1.42 0.7 -0.31 Arsenic -0.18 1. -0.400, 1.0 23.4 25.0 93.8 23.8 25.0 95.4 1.71 0.7 -0.090 Barium 0.0050 5. 0.0 5.0 25.1 25. 100,24.7 25.0 98.6 1.87, 3.5 0.024 Beryllium 0.0050 0.1 0.0 0.1 24.4 25. 97.7 24.0 25.0 95.9 1.86 0.070 0.0 Cadmium 0.0050 0.2 0.0 0.2 26.6 25. 107 24.4 25.0 97.7 8.68 0.14 0.0034 Chromium -0.010 1. 0.010 1. 25.3 25. 101 25.3 25.0 101 0.0989 0.70 0.027 Cobalt -0.010 0.5 -0.0050 0.5 27.3 25. 109 27.1 25.0 108 1.01 0.3 -0.0034 Copper -0.0050 1. -0.010 1. 26.7 25. 107 26.4 25.0 106 1.11 0.70 0.18 Lead 0.0750 0.5 -0.045 0.50 25.3 25. 101 24.9 25.0 99.6 1.40 0.35 0.010 Manganese -0.0050 0.5 -0.0050 0.50 25.3 25. 101 25.1 25.0 100 0.893 0.35 0.010 Molybdenum 0.0100 0.50 0.030 0.50 26.6 25.0 106 26.2 25.0 105 1.38 0.35 0.017 Nickel -0.00500 1.0 0.010 1.0 25.7 25. 103 25.5 25.0 102 0.702 0.70 0.024 Selenium -0.77 1. -0.225 1.0 23.9 25. 95.8 23.5 25.0 94.1 1.71 0.7 -0.20 Silver 0.020 1. -0.010 1. 25.7 25.q 103 25.5 25.0 102 0.87q 0.7 -0.0069 Thallium -0.30 1. -0.11 1. 26.1 25. 105 25.9 25.0 104 0.749 0.7 -0.13 Vanadium 0.0250 0.5 -0.020 0.5 25.7 25. 103 25.5 25.0 102 0.469 0.3 -0.010 Zinc 0.015q 1.0 0.030 1. 27.1 25. 109 26.9 25.0 107 1.68 0.70 0.16 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 1 of 2 Page 22 Of 30 Printed: 4/1 /2024 Batch: 33Q240328-2MC E Instrument: 33-PE8300 Initial Cal Std: Cal Check Std: Internal Std: LCS Std MS Std Matrix: Cassettes Other 332405230-0022 03/29/24 11:15 RL pg/filter Result pg/filter Aluminum 5. 0.24 Antimony 1. -0.34 Arsenic 1. -0.31 Barium 5.0 0.015 Beryllium 0.10 0.0 Cadmium 0.20 0.010 Chromium 1.0 0.045 Cobalt 0.5 -0.030 Copper 1.0 0.23 Lead 0.5 -0.10 Manganese 0.50 0.015 Molybdenum 0.50 0.025 Nickel 1.0 0.020 Selenium 1. -0.36 Silver 1.0 0.025 Thallium 1. -0.24 Vanadium 0.50 0.0 Zinc 1.0 0.20 ICP QC Batch Summary Created: 3/28/24 11:26 am By: camartinez 332404864-0001 332404864-0005 332405230-0022 332405564-0004 332405564-0008 332404864-0002 332404864-0006 332405564-0001 332405564-0005 332405564-0009 332404864-0003 332404864-0007 332405564-0002 332405564-0006 332405564-0010 332404864-0004 332405230-0021 332405564-0003 332405564-0007 (') Result outside control limits (#) Sample Result > 4 x spike amt (x) No solids data CHEMICPBATSUMX 3.0 Page 2 of 2 Page 23 Of 30 OrderID: 332405230 m r c m I v _ m C � �rn 1 m f'? 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Page 26 Of 30 I Y 1 11 x Paae 3 Of 3 =r a o a (D LA LA a o m 3 00 z a oaf n� 0 � n S� m O m n Z O A s ro O n X D m V N 00 r, d ❑c El 2 o orti � • o ro o m m o m ro �n,a�� a �c x m c m o � EL A ro m r_r ems+ 2L S� ro �mp a 0 @ '� ■ -,c ❑ W 3 K f1 Z N X pi O S d 0 7 rL ~ m d �• H n m m m m y ro ❑ v 0 m ❑ m v a 1 l J n_ z 0 mn n 0 v z v z V1 m m 0 m LA Testing 5431 Industrial Drive, Huntington Beach, CA 92649 /Pir Phone: (714) 828-4999 Fax: (714) 828-4944 I Email: hblab@latesting.com TESTING Attn: Noah Ambos Customer ID: CTEH99 CTEH Center for Toxicology & Env. Health Customer PO: 5120 North Shore Drive Received: 03/22/24 10:35 AM North Little Rock, AR 72118 Fax: (501) 614-2835 Phone: (501) 454-1622 LA Testing Order: 332405230 Project: PRO7-032229 LA Testing Proj ID: PROJ-032229 Cust COC ID Project Type: Standard Project Receipt Confirmation Shipping Tracking Number: EMSL Received Cust Sample Order ID Test Date TAT Due Date TUCA0321ME001A 332405230-0001 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321ME001A 332405230-0001 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME002A 332405230-0002 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME002A 332405230-0002 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME003A 332405230-0003 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME003A 332405230-0003 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME004A 332405230-0004 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME004A 332405230-0004 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME005A 332405230-0005 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME005A 332405230-0005 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME006A 332405230-0006 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME006A 332405230-0006 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME007A 332405230-0007 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM Date Sent 312212024 2:41:43 PM Paqe 27 Of 30 1 911ALA Testing 5431 Industrial Drive, Huntington Beach, CA 92649 Phone: (714) 828-4999 Fax: (714) 828-4944 Email: hblab@latesting.com TESTING Attn: Noah Ambos Customer ID: CTEH99 CTEH Center for Toxicology & Env. Health Customer PO: 5120 North Shore Drive North Little Rock, AR 72118 Received: 03/22/24 10:35 AM Fax: (501) 614-2835 Phone: (501) 454-1622 LA Testing Order: 332405230 Project: PRO7-032229 LA Testing Proj ID: PROJ-032229 Cust COC ID Project Type: Standard Project Receipt Confirmation Shipping Tracking Number: EMSL Received Cust Sample Order ID Test Date TAT Due Date TUCA0321 ME007A 332405230-0007 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME008A 332405230-0008 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME008A 332405230-0008 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME009A 332405230-0009 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME009A 332405230-0009 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME010A 332405230-0010 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME010A 332405230-0010 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321MEFBO01A 332405230-0011 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321MEFBO01A 332405230-0011 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321ME001B 332405230-0012 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321ME001B 332405230-0012 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME002B 332405230-0013 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME002B 332405230-0013 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM Date Sent 312212024 2:41:43 PM Paqe 28 Of 30 2 911ALA Testing 5431 Industrial Drive, Huntington Beach, CA 92649 Phone: (714) 828-4999 Fax: (714) 828-4944 Email: hblab@latesting.com TESTING Attn: Noah Ambos Customer ID: CTEH99 CTEH Center for Toxicology & Env. Health Customer PO: 5120 North Shore Drive North Little Rock, AR 72118 Received: 03/22/24 10:35 AM Fax: (501) 614-2835 Phone: (501) 454-1622 LA Testing Order: 332405230 Project: PRO7-032229 LA Testing Proj ID: PROJ-032229 Cust COC ID Project Type: Standard Project Receipt Confirmation Shipping Tracking Number: EMSL Received Cust Sample Order ID Test Date TAT Due Date TUCA0321 ME003B 332405230-0014 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME003B 332405230-0014 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME004B 332405230-0015 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME004B 332405230-0015 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME005B 332405230-0016 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME005B 332405230-0016 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME006B 332405230-0017 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME006B 332405230-0017 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME007B 332405230-0018 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME007B 332405230-0018 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME008B 332405230-0019 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME008B 332405230-0019 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME009B 332405230-0020 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM Date Sent 312212024 2:41:43 PM Paqe 29 Of 30 3 911ALA Testing 5431 Industrial Drive, Huntington Beach, CA 92649 Phone: (714) 828-4999 Fax: (714) 828-4944 Email: hblab@latesting.com TESTING Attn: Noah Ambos Customer ID: CTEH99 CTEH Center for Toxicology & Env. Health Customer PO: 5120 North Shore Drive North Little Rock, AR 72118 Received: 03/22/24 10:35 AM Fax: (501) 614-2835 Phone: (501) 454-1622 LA Testing Order: 332405230 Project: PRO7-032229 LA Testing Proj ID: PROJ-032229 Cust COC ID Project Type: Standard Project Receipt Confirmation Shipping Tracking Number: EMSL Received Cust Sample Order ID Test Date TAT Due Date TUCA0321 ME009B 332405230-0020 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME010B 332405230-0021 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321 ME010B 332405230-0021 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321MEFBO01B 332405230-0022 C-CAM 16 Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM TUCA0321MEFBO01B 332405230-0022 C-Metals by ICP 3/22/2024 1 Week (EOD) 3/29/2024 10:35:00 AM 6:00:00 PM Note: The above sample log -in information is based solely on the data provided by the customer on the Chain of Custody form. Sample count, ID number verification, and evaluation of each individual sample is not started/done until sample analysis process begins by the scientist at the lab bench. If at this point the staff finds that a sample is missing, ID number does not match, or has any other issue that will disrupt analysis, the customer will be notified. Date Sent 312212024 2:41:44 PM Paqe 30 Of 30 4